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GCMS analysis results for sample AE00838, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00838 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050411–000050420

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050415
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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00838.D Vial: 7 Acq On : 23 Jan 2002 7:54 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.488 5 10 13 rBV 23365 37158 0.30% 0.056% 2 3.613 17 21 25 rVB 31934 47281 0.38% 0.071% 3 3.922 45 48 53 rVB 14624 26472 0.21% 0.040% 4 4.241 73 76 85 rVB3 9829 27520 0.22% 0.041% 5 6.011 227 231 235 rBV 15873 27512 0.22% 0.041% 6 9.550 537 541 547 rBV3 12889 38109 0.30% 0.057% 7 9.641 547 549 551 rW 14672 30390 0.24% 0.046% 8 9.710 551 555 561 rW 3902815 7720073 61.57% 11.568% 9 9.847 561 567 577 rVB2 20645 72767 0.58% 0.109% 10 10.212 589 599 609 rVB3 4269 27382 0.22% 0.041% 11 13.192 855 860 865 rBV 5528296 10913130 87.04% 16.352% 12 18.341 1305 1311 1315 rBV 5810328 11713955 93.43% 17.552% 13 22.280 1651 1656 1661 rBV 47626 88331 0.70% 0.132% 14 22.645 1681 1688 1693 rBV2 5505579 12538303 100.00% 18.787% 15 22.771 1695 1699 1715 rVB 72403 224848 1.79% 0.337% 16 24.849 1877 1881 1885 rBV 34198 62205 0.50% 0.093% 17 27.726 2127 2133 2139 rBV 850205 1496786 11.94% 2.243% 18 30.500 2369 2376 2381 rBV 4655834 11603671 92.55% 17.387% 19 31.105 2419 2429 2443 rW2 27761 120078 0.96% 0.180% 20 34.416 2713 2719 2755 rBV 3589013 9921636 79.13% 14.867%

Sum of corrected areas: 66737607

00838.D SCAN508.M Thu Jan 24 09:57:25 2002 Page 1

NYC-WTC_000050415

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NYC-WTC_000050415Source: NYC Law Department, mirrored locally

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