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GCMS analysis results for sample AD31646, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050240–000050257

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31646.D Vial: 2 Acq On : 22 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.476 5 9 15 rVB 16313 36394 0.34% 0.062% 2 3.602 15 20 25 rBV 36209 64221 0.61% 0.110% 3 4.367 83 87 91 rBV 42593 78609 0.74% 0.135% 4 6.000 225 230 235 rBV2 17221 32076 0.30% 0.055% 5 9.447 527 532 537 rVB2 14237 42730 0.40% 0.073% 6 9.539 537 540 545 rBV 34034 79898 0.76% 0.137% 7 9.630 545 548 551 rW 36649 85477 0.81% 0.147% 8 9.710 551 555 563 rW 3161402 6424934 60.72% 11.027% 9 9.836 563 566 581 rVB 33686 107684 1.02% 0.185% 10 12.541 799 803 809 rVB 23760 39855 0.38% 0.068% 11 13.192 855 860 865 rBV 4793108 9042504 85.45% 15.520% 12 18.341 1305 1311 1315 rBV 4908791 9773946 92.37% 16.775% 13 22.280 1653 1656 1661 rVB2 38844 70052 0.66% 0.120% 14 22.634 1681 1687 1693 rBV2 4902088 10581670 100.00% 18.162% 15 22.771 1695 1699 1707 rVB2 56791 153226 1.45% 0.263% 16 24.849 1877 1881 1887 rW 113155 202118 1.91% 0.347% 17 26.013 1977 1983 1987 rBV 399008 733950 6.94% 1.260% 18 27.726 2127 2133 2137 rBV 795391 1446151 13.67% 2.482% 19 30.489 2369 2375 2381 rBV2 4376157 10344775 97.76% 17.755% 20 34.416 2713 2719 2743 rBV 3292851 8923139 84.33% 15.315%

Sum of corrected areas: 58263409

31646.D SCAN508.M Thu Jan 24 13:55:33 2002 Page 1

NYC-WTC_000050244

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NYC-WTC_000050244Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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