GCMS analysis results for sample AE00832, Feb 4 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00832.D Vial: 5 Acq On : 31 Jan 2002 1 : 52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.920 221 223 231 rBV 120299 260772 0.76% 0.198% 2 6.034 231 233 247 rVB 100656 267486 0.78% 0.203% 3 7.153 327 331 341 rBV3 13309 113473 0.33% 0.086% 4 9.710 551 555 561 rW 5771764 10978976 31.83% 8.338% 5 9.858 561 568 587 rW2 21384 129219 0.37% 0.098%

6 13.192 855 860 865 rBV 7761914 15791972 45.78% 11.994% 7 13.409 873 879 885 rBV2 135591 273983 0.79% 0.208% 8 15.190 1031 1035 1039 rW 132503 239228 0.69% 0.182% 9 16.868 1177 1182 1185 rW 65933 127755 0.37% 0.097% 10 18.341 1305 1311 1315 rBV 7989770 17135605 49.68% 13.014%

11 18.433 1315 1319 1325 rVB2 66967 168472 0.49% 0.128% 12 22.280 1651 1656 1661 rW 88419 166936 0.48% 0.127% 13 22.645 1681 1688 1693 rBV2 7561984 17844202 51.73% 13.552% 14 22.771 1695 1699 1719 rVB 106513 342900 0.99% 0.260% 15 24.723 1865 1870 1877 rBV 82723 200160 0.58% 0.152%

16 27.052 2069 2074 2077 rBV 146522 325165 0.94% 0.247% 17 27.726 2127 2133 2137 rBV 1151595 2240936 6.50% 1.702% 18 30.500 2369 2376 2381 rBV 6429348 16502271 47.84% 12.533% 19 33.423 2625 2632 2683 rBV 9656824 34492253 100.00% 26.196% 20 34.416 2713 2719 2753 rVB2 4947801 14066023 40.78% 10.683%

Sum of corrected areas: 131667787

00832. D SCAN508.M Fri Feb 01 09:18:51 2002 Page 1

NYC-WTC_000052151