GCMS results for sample AE00463, Jan 24 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00463.D Vial: 5 Acq On : 11 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C: \MSDCHEM\1\METHODS\METHODS\SCAN508 .M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rVB 27471 41383 0.37% 0.068% 2 4.630 107 110 117 rVB3 12358 29919 0.27% 0.049% 3 4.847 123 129 139 rBV3 13770 44770 0.40% 0.073% 4 5.006 139 143 14 9 rW 67005 110595 0.98% 0.181% 5 5.520 185 188 201 rVB3 7385 28112 0.25% 0.046%

6 5.703 201 204 209 rBV 36727 70724 0.63% 0.116% 7 5.885 215 220 245 rBV 783256 1586890 14.13% 2.598% 8 9.550 537 541 547 rBV2 13833 33505 0.30% 0.055% 9 9.642 547 549 551 rW 15801 31452 0.28% 0.051% 10 9.710 551 555 561 rW 3094556 6229229 55.45% 10.199%

11 9.847 561 567 577 rVB 19357 64052 0.57% 0.105% 12 13.192 855 860 865 rBV 4755317 8932287 79.51% 14.624% 13 18.341 1305 1311 1315 rBV 5173844 10176151 90.58% 16.661% 14 22.280 1651 1656 1661 rBV2 40581 76814 0.68% 0.126% 15 22.634 1681 1687 1693 rBV2 4978341 11233914 100.00% 18.392%

16 22.771 1695 1699 1707 rVB 61276 155189 1.38% 0.254% 17 27.726 2129 2133 2139 rW 824425 1475662 13.14% 2.416% 18 30.489 2369 2375 2381 rBV 4472037 10964889 97.61% 17.952% 19 33.400 2625 2630 2645 rBV 105206 434753 3.87% 0.712% 20 34.416 2713 2719 2755 rBV 3737645 9358569 83.31% 15.322%

Sum of corrected areas: 61078859

00463.D SCAN508.M Mon Jan 14 10:46:55 2002 Page 1

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