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GCMS results for sample AE00464, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00464 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051439–000051452

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051443
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LsC Area Percent Keport

Data File : C:\MSDCHEM\1\5973N\02JAN11\00464.D Vial: 6 Acq Cn : 11 Jan 2002 6:15 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.614 19 21 25 rBV 20968 36015 0.35% 0.062% 2 4.858 125 130 141 rBV4 12470 47105 0.45% 0.081% 3 5.006 141 143 153 rVB 50811 92081 0.89% 0.158% 4 5.714 199 205 209 rBV 31988 60621 0.58% 0.104% 5 5.885 217 220 245 rVB 614607 1416707 13.66% 2.436%

6 9.710 551 555 563 rW 3073265 6368163 61.42% 10.950% 7 9.847 563 567 577 rW 15420 50849 0.49% 0.087% 8 13.192 855 860 865 rBV 4759398 9049902 87.28% 15.561% 9 18.341 1305 1311 1315 rBV 5008776 9717040 93.72% 16.708% 10 22.280 1651 1656 1661 rBV 40034 73020 0.70% 0.126%

11 22.634 1681 1687 1693 rBV2 4698242 10329523 99.63% 17.761% 12 22.771 1695 1699 1709 rVB 55001 133072 1.28% 0.229% 13 24.849 1877 1881 1887 rW 46159 84344 0.81% 0.145% 14 27.726 2129 2133 2139 rBV 726213 1267682 12.23% 2.180% 15 29.244 2261 2266 2277 rVB 16574 40989 0.40% 0.070%

16 30.489 2369 2375 2381 rBV2 4264078 10368227 100.00% 17.828% 17 31.105 2425 2429 2443 rVB2 25714 102304 0.99% 0.176% 18 33.446 2629 2634 2635 rW 18319 42908 0.41% 0.074% 19 33.503 2635 2639 2653 rVB3 24784 109912 1.06% 0.189% 20 34.416 2713 2719 2749 rBV 3560797 8767385 84.56% 15.075%

Sum of corrected areas: 58157849

00464.D SCAN508.M Mon Jan 14 10:47:00 2002 Page 1

NYC-WTC_000051443

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NYC-WTC_000051443Source: NYC Law Department, mirrored locally

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