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GCMS analysis results for sample AE00320, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00320 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051137–000051151

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document LSC Area Percent Keport

Data File : C:\MSDCHEM\1\5973N\02JAN08\320.D Vial: 5 Acq On : 8 Jan 2002 8:47 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.476 7 9 17 rVB 16852 31029 0.27% 0.049% 2 3.602 17 20 25 rBV 34458 57882 0.50% 0.091% 3 3.990 51 54 67 rW 11496 32738 0.28% 0.052% 4 4.230 73 75 83 rVB3 14293 38076 0.33% 0.060% 5 4.618 107 109 125 rVB3 15626 43792 0.38% 0.069%

6 4.846 125 129 141 rBV4 19093 68122 0.59% 0.107% 7 5.006 141 143 149 rVB 29512 57295 0.49% 0.090% 8 5.234 159 163 169 rVB2 17451 33517 0.29% 0.053% 9 5.885 217 220 247 rBV 804500 1884357 16.23% 2.969% 10 9.710 551 555 561 rW 3356692 6920869 59.59% 10.905%

11 13.192 855 860 865 rBV 5289839 9874074 85.02% 15.559% 12 18.341 1305 1311 1315 rBV 5704470 10791919 92.93% 17.005% 13 22.280 1651 1656 1661 rBV 41554 76125 0.66% 0.120% 14 22.645 1681 1688 1693 rBV 5238864 11613392 100.00% 18.299% 15 22.771 1695 1699 1711 rVB 65576 177608 1.53% 0.280%

16 27.543 2113 2117 2121 rW2 25906 50344 0.43% 0.079% 17 27.726 2129 2133 2139 rBV 987894 1755941 15.12% 2.767% 18 30.489 2369 2375 2381 rBV2 4587711 10867199 93.57% 17.124% 19 31.105 2425 2429 2443 rVB 22379 70118 0.60% 0.110% 20 34.416 2713 2719 2745 rBV 3630509 9019125 77.66% 14.212%

Sum of corrected areas: 63463522

320.D SCAN508.M Wed Jan 09 15:18:11 2002 Page 1

NYC-WTC_000051141

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