GCMS analysis results for sample AE00309, Jan 2002

NYC 9/11 Public Portal Document

LSC Area percent Keport

Data File : C : \MSDCHEM\1\5973N\02JAN08\309 .D Vial: 8 Acq On : 8 J an 2 002 11:19 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rBV 28251 42624 0.38% 0.070% 2 4.241 73 76 83 rBV2 17124 40899 0.37% 0.067% 3 4.618 107 109 121 rVB3 16136 44189 0.39% 0.072% 4 4.835 123 128 141 rBV3 22787 77518 0.69% 0.127% 5 5.006 141 143 147 rVB 24156 41048 0.37% 0.067%

6 5.703 199 204 209 rW 15509 32348 0.29% 0.053% 7 5.885 217 220 231 rW 753990 1547353 13.83% 2.531% 8 6.045 231 234 253 rVB 31715 103965 0.93% 0.170% 9 9.710 551 555 561 rW 3228367 6396168 57.16% 10.463% 10 13.192 855 860 865 rBV 4983373 9229469 82.49% 15.097%

11 18.341 1305 1311 1315 rBV 5291051 10111831 90.37% 16.540% 12 19.962 1445 1453 1465 rVB4 4898 26579 0.24% 0.043% 13 22.280 1653 1656 1661 rBV 43227 83389 0.75% 0.136% 14 22.645 1681 1688 1693 rBV2 4941420 11124157 99.42% 18.196% 15 22.771 1697 1699 1707 rVB 57103 124908 1.12% 0.204%

16 27.532 2113 2116 2123 rBV2 16558 40825 0.36% 0.067% 17 27.726 2129 2133 2139 rW 1009062 1801885 16.10% 2.947% 18 30.489 2369 2375 2381 rBV2 4700561 11189178 100.00% 18.303% 19 31.105 2427 2429 2439 rVB4 10725 30161 0.27% 0.049% 20 34.416 2713 2719 2743 rBV 3582815 9045725 80.84% 14.797%

Sum of corrected areas: 61134219

309.D SCAN508.M Wed Jan 09 15:17:25 2002 Page 1

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