GCMS analysis results for sample AE00308, Jan 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN08\308.D Vial : 7 Acq On : 8 Jan 2002 10:28 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.591 15 19 25 rBV 22040 36141 0.34% 0.061% 2 4.241 71 76 83 rW2 15360 39072 0.37% 0.066% 3 4.618 107 109 115 rBV2 17344 39314 0.37% 0.067% 4 4.835 125 128 137 rBV2 28370 78046 0.73% 0.133% 5 4.995 137 142 153 rVB4 19564 46061 0.43% 0.078%

6 5.703 199 204 209 rVB3 16091 31013 0.29% 0.053% 7 5.885 215 220 247 rVB 633562 1478341 13.88% 2.514% 8 9.653 539 550 551 rBV5 6473 24365 0.23% 0.041% 9 9.710 551 555 563 rW 3168448 6552007 61.53% 11.143% 10 12.541 799 803 807 rBV 14210 22007 0.21% 0.037%

11 13.192 855 860 865 rBV 4959321 9331856 87.63% 15.871% 12 16.549 1151 1154 1159 rBV 11857 22893 0.21% 0.039% 13 18.341 1305 1311 1315 rBV 5372937 10136301 95.19% 17.239% 14 22.280 1651 1656 1661 rBV 38297 69183 0.65% 0.118% 15 22.634 1681 1687 1693 rW2 4784889 10648659 100.00% 18.111%

16 22.771 1695 1699 1711 rVB 55119 158528 1.49% 0.270% 17 27.726 2129 2133 2139 rBV 839118 1449615 13.61% 2.465% 18 30.489 2369 2375 2381 rBV2 4419686 10263312 96.38% 17.455% 19 31.105 2425 2429 2439 rW2 10307 32026 0.30% 0.054% 20 34.416 2713 2719 2739 rBV 3344714 8339520 78.32% 14.183%

Sum of corrected areas: 58798260

308.D SCAN508.M Wed Jan 09 15:17:07 2002 Page 1

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