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GCMS analysis results for sample AE00307, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051055–000051072

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C : \MSDCHEM\1\5973N\02JAN08\307.D Vial: 6 ' Acq On : 8 Jan 2002 9:37 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.602 15 20 25 rBV 32219 50026 0.45% 0.082% 2 4.241 71 76 83 rVB4 22806 52429 0.47% 0.086% 3 4.618 107 109 123 rW3 23763 55291 0.50% 0.091% 4 4.835 123 128 13 9 rW2 32390 109767 0.99% 0.181% 5 5.006 139 143 151 rVB 27670 52238 0.47% 0.086%

6 5.703 201 204 209 rBV2 19614 36510 0.33% 0.060% 7 5.885 215 220 233 rW 791920 1668136 14.97% 2.747% 8 6.045 233 234 247 rVB2 21194 63467 0.57% 0.105% 9 9.710 551 555 561 rW 3217262 6604558 59.28% 10.876% 10 9.847 561 567 577 rVB 14733 42091 0.38% 0.069%

11 12.541 799 803 807 rBV 25653 40416 0.36% 0.067% 12 13.192 855 860 865 rBV 4989502 9268032 83.18% 15.263% 13 18.341 1305 1311 1315 rBV 5132890 9902384 88.87% 16.307% 14 22.280 1651 1656 1661 rBV2 36506 71119 0.64% 0.117% 15 22.634 1681 1687 1693 rBV2 4824977 10658514 95.66% 17.552%

16 22.771 1695 1699 1711 rVB 56665 157875 1.42% 0.260% 17 27.726 2129 2133 2139 rVB 890529 1570117 14.09% 2.586% 18 30.489 2369 2375 2381 rBV2 4644157 11142112 100.00% 18.349% 19 31.105 2421 2429 2439 rBV5 14493 59744 0.54% 0.098% 20 34.416 2713 2719 2743 rW 3657949 9118884 81.84% 15.017%

Sum of corrected areas: 60723710

307.D SCAN508.M Wed Jan 09 15:16:55 2002 Page 1

NYC-WTC_000051059

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NYC-WTC_000051059Source: NYC Law Department, mirrored locally

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