GCMS analysis results for sample AD31670, Jan 28 2002

NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31670.D Vial: 5 ' Acq On : 17 Jan 2002 6:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total- 1 3.614 17 21 25 rBV 48524 73193 0.51% 0.092% 2 4.241 69 76 81 rW2 51722 108944 0.77% 0.136% 3 4.630 103 110 119 rVB3 31640 72700 0.51% 0.091% 4 4.835 123 128 139 rVB 44872 127994 0.90% 0.160% 5 5.886 215 220 249 rVB 1074391 ' 1987457 13.97% 2.490%

6 9.539 537 540 545 rW5 21571 50571 0.36% 0.063% 7 9.630 545 548 551 rW 26238 53242 0.37% 0.067% 8 9.710 551 555 561 rW 4638949 8791533 61.79% 11.015% 9 9.836 561 566 575 rW 25905 83725 0.59% 0.105% 10 13.192 855 860 865 rBV 6319734 12372467 86.96% 15.501%

11 18.341 1305 1311 1315 rBV 6385797 13326543 93.66% 16.696% 12 21.333 1569 1573 1577 rBV 27400 47522 0.33% 0.060% 13 22.280 1653 1656 1661 rBV2 58186 106574 0.75% 0.134% 14 22.646 1681 1688 1693 rBV2 6213440 14228104 100.00% 17.826% 15 22.771 1695 1699 1707 rVB 84406 205113 1.44% 0.257%

16 24.027 1805 1809 1823 rVB 15547 48173 0.34% 0.060% 17 24.849 1877 1881 1889 rVB 154117 282226 1.98% 0.354% 18 27.726 2127 2133 2139 rBV 1138793 2014962 14.16% 2.524% 19 30.500 2369 2376 2381 rBV 5517028 13903588 97.72% 17.419% 20 34.416 2713 2719 2751 rBV2 4301091 11932474 83.87% 14.950%

Sum of corrected areas: 79817105

31670.D SCAN508.M Tue Jan 22 08:37:21 2002 Page 1

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