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GCMS analysis results for sample AE00276, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00276 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051040–000051054

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\5973N\02JAN08\276.D Vial: 1 Acq On : 8 Jan 2002 5:26 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.476 5 9 17 rVB 18251 36550 0.28% 0.051% 2 3.602 17 20 25 rBV 38532 59531 0.45% 0.083% 3 3.979 49 53 57 rW3 17702 34676 0.26% 0.049% 4 4.618 107 109 125 rW2 20525 48791 0.37% 0.068% 5 4.835 125 128 13 9 rW2 28108 84782 0.64% 0.119%

6 5.006 139 143 149 rVB 47028 80862 0.62% 0.113% 7 5.703 201 204 209 rW 27369 43682 0.33% 0.061% 8 5.874 217 219 245 rBV 989765 2208653 16.80% 3.089% 9 9.710 551 555 561 rW 4016027 7319563 55.68% 10.238% 10 12.542 799 803 813 rVB 19740 38478 0.29% 0.054%

11 13.192 855 860 865 rBV 5760950 10484526 79.75% 14.665% 12 18.341 1305 1311 1315 rBV 5930510 11446829 87.07% 16.011% 13 19.951 1447 1452 1457 rW2 17943 46086 0.35% 0.064% 14 22.280 1653 1656 1661 rBV2 45379 85354 0.65% 0.119% 15 22.645 1681 1688 1693 rBV2 5793174 12672564 96.39% 17.726%

16 22.771 1695 1699 1711 rVB2 66844 189396 1.44% 0.265% 17 27.726 2129 2133 2139 rBV 1151239 2133983 16.23% 2.985% 18 30.500 2369 2376 2381 rBV2 5532271 13146849 100.00% 18.389% 19 31.105 2427 2429 2437 rVB3 18259 48170 0.37% 0.067% 20 34.416 2713 2719 2725 rBV2 4396366 11282379 85.82% 15.781%

Sum of corrected areas: 71491704

276. D SCAN508.M Wed Jan 09 15:16:15 2002 Page 1

NYC-WTC_000051044

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NYC-WTC_000051044Source: NYC Law Department, mirrored locally

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