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GCMS analysis results for sample AE00248, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00248 analyzed on January 28, 2002.

NYC-WTC_000050558–000050576

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN24\00248.D Vial: 4 Acq On : 24 Jan 2002 5:27 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0' Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.614 17 21 25 rBV 44460 62064 0.40% 0.072% 2 3.922 45 48 53 rVB2 20829 32465 0.21% 0.038% 3 4.253 73 77 81 rBV 31548 60283 0.39% 0.070% 4 4.630 107 110 123 rVB3 24680 50719 0.33% 0.059% 5 4.847 123 129 141 rVB2 28859 75814 0.49% 0.088%

6 5.018 141 144 149 rBV 81658 144960 0.94% 0.168% 7 5.714 201 205 209 rVB 60592 93791 0.61% 0.109% 8 5.885 217 220 253 rVB 1030717 2115814 13.69% 2.455% 9 9.722 551 556 561 rBV 4997271 9974998 64.56% 11.572% 10 12.542 799 803 807 rBV 28844 47808 0.31% 0.055% 11 13.192 855 860 865 rBV 6808469 14127656 91.44% 16.389% 12 16.549 1149 1154 1159 rW 15919 33277 0.22% 0.039% 13 18.341 1305 1311 1315 rBV 7302809 14825463 95.96% 17.199% 14 22.280 1653 1656 1661 rBV2 63237 121442 0.79% 0.141% 15 22.646 1681 1688 1693 rBV2 6931752 15450271 100.00% 17.924%

16 22.771 1697 1699 1717 rW 95117 270267 1.75% 0.314% 17 27.726 2127 2133 2139 rBV 947583 1744116 11.29% 2.023% 18 30.500 2369 2376 2381 rBV 6011361 14420720 93.34% 16.729% 19 31.105 2421 2429 2439 rBV4 31975 133934 0.87% 0.155% 20 34.416 2713 2719 2749 rBV 4486985 12414596 80.35% 14.402%

Sum of corrected areas: 86200458

00248.D SCAN508.M Fri Jan 25 10:26:09 2002 Page 1

NYC-WTC_000050562

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