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GCMS analysis results for sample AE00249, Jan 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.

NYC-WTC_000050577–000050595

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document LSC Area Percent Report . Data File : C:\MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq On : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 4.847 125 129 141 rBV2 20617 72398 0.48% 0.090% 2 5.006 141 143 153 rVB 83160 152734 1.02% 0.189% 3 5.714 199 205 209 rW 52476 94819 0.63% 0.117% 4 5.885 217 220 243 rVB 873262 1887096 12.62% 2.338% 5 9.722 551 556 561 rBV 4258674 8600016 57.52% 10.655% 6 13.192 855 860 865 rBV 6253590 12328530 82.46% 15.275% 7 18.341 1305 1311 1315 rBV 6953312 13598038 90.95% 16.847% 8 22.280 1651 1656 1661 rBV 57369 103730 0.69% 0.129% 9 22.645 1681 1688 1693 rBV2 6770203 14950777 100.00% 18.523% 10 22.771 1697 1699 1707 rVB 89544 183890 1.23% 0.228% 11 27.726 2129 2133 2139 rBV 929907 1616093 10.81% 2.002% 12 30.500 2369 2376 2381 rBV 5757991 14043576 93.93% 17.399% 13 31.105 2423 2429 2443 rBV 35991 156696 1.05% 0.194% 14 32.384 2535 2541 2551 rBV3 18933 69469 0.46% 0.086% 15 33.263 2613 2618 2627 rBV 46295 141987 0.95% 0.176% 16 34.119 2687 2693 2713 rBV 66138 272621 1.82% 0.338% 17 34.416 2713 2719 2757 rW 4370532 12018788 80.39% 14.891% 18 34.941 2761 2765 2789 rW 58865 227894 1.52% 0.282% 19 35.741 2829 2835 2839 rBV 47470 116671 0.78% 0.145% 20 36.608 2905 2911 2919 rBV3 21767 77138 0.52% 0.096%

Sum of corrected areas: 80712961

)0249.D SCAN508.M Fri Jan 25 10:26:16 2002 Page 1

NYC-WTC_000050581

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