GCMS surrogate recovery results for sample AE00317, Jan 2002

NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\l\5973N\02JAN10\00317 .D Vial : 4 Acq On : 10 Jan 2002 10:57 am Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 2 (E)-1-Propenylaziridine $$ ... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.85 0.16 ug/L 52005 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 (E)-1-Propenylaziridine $$ Aziri... 83 C5H9N 080839-91-4 9 2 Cyclobutaneethanol, .beta.-methy... 112 C7H120 116203-80-6 9 3 Pyridine, 2,3,4,5-tetrahydro- $$... 83 C5H9N 000505-18-0 7 4 2-Butenal, 2-methyl- (CAS) $$ 2-... 84 C5H80 001115-11-3 5 Abundance Scan 129 (4.846 min): 00317.D (-) m/ z 84.00 100.00% 84 55

5000 39

44 4.40 4.60 4.80 5.00' 5.20 ' Of rI" " I i " i" m/z 55.10 71.90% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #3037: (E)-1-Propenylaziridine $$ Aziridine, 1-(1-propenyl... 41 55 83

5000 27 Tr —N "'J. I A-— 4.40 4.60 4.80 5.00। 5.20 68 m/Z 83.10 !58.25%

n/z-> 0 TH''1 I 1 ‘ r1" I1" ml Im +TmTTTUTTTTTTTTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #13627: Cyclobutaneethanol, beta.-methylene- 55 84 ■ i ' ■ • > i • ’ ■ 440 4.60 4.80 5.00 5.20 5000 m/z 59.10 44.21% 41 69 79

/z-> 0 -T -LL. ’’I’ 112 । • > > ■ । • • •»I" ‘ • i" " i" " i ■1 ■ ■ i" " i ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #3044: Pyridine, 2,3,4,5-tetrahydro- $$ .delta. 1-Piperidei... ...A -- 55 4.40 4.60 4.80 5.001 5.20 m/z 39.10 43,68% 83 A 5000 41 27

0 ’" I" —HP ...... —1 mm 68 — i" "r " ‘ i" " i" " i" " i /z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 4.40 4.60 4.80 5.00 5.20

30317.D SCAN508.M Thu Jan 10 11:52:16 2002 Page 4

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