GCMS analysis results for sample AE00110, Feb 2002

NYC 9/11 Public Portal Document y *•— 1 ASV.LSWS/

Data File : C:\MSDCHEM\1\5973N\02FEB04\0204RB.D Vial: 2 . Acq On : 4 Feb 2002 11:48 am Operator: Sample : ref l/4b Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 05 08:28:41 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1987441 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 8493279. 20.00 ug/L -0.01 17) Acenaphthene-dl0 18.34 164 4359661- 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 6984035 20.00 ug/L -0.02 38) Chrysene-dl2 30.51 240 6085396 20.00 ug/L 0.00 44) Perylene-dl2 34.43 264 4383041 20.00 ug/L 0.01 System Monitoring Compounds 37) 2,4-DDD 27.73 235 405087 3.67 ug/L 0.00 Spiked Amount 5.000 Recovery = 73.40% Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.00 74 183528 2.17 ug/L 49 3) bis(2-Chloroethyl)ether 9.24 93 473687 3.37 ug/L 68 4) 1,3-Dichlorobenzene 9.61 146 301007 2.02 ug/L 96 5) 1,4-Dichlorobenzene 9.76 146 316044 2.11 ug/L 97 6) 1,2-Dichlorobenzene 10.24 146 328088 2.47 ug/L 99 7) 2,2'-oxybi s (1-Chioropropa 10.67 45 658964 2.87 ug/L # 73 8) n-Nitroso-di-n-propylamine 11.06 70 314897 3.00 ug/L 73 9) Hexachloroethane 11.03 117 72370 1.35 ug/L 96 11) Nitrobenzene 11.35 77 396073 2.50 ug/L 83 12) 1sophorone 12.03 82 898178 3.14 ug/L 92 13) bis(2-Chloroethoxy)methane 12.77 93 580962 3.42 ug/L 91 14) 1,2,4-Trichlorobenzene 13.11 180 265090 2.39 ug/L 96 15) Naphthalene 13.25 128 1287777 3.17 ug/L 98 16) Hexachiorobutadiene 13.84 225 70090 1.19 ug/L 99 18) Hexachlorocyclopentadiene 15.96 237 10637 0.27 ug/L 92 19) 2-Chloronaphthalene 16.65 162 714827 2.97 ug/L 93 20) Dimethylphthalate 17.88 163 957749 3.33 ug/L 95 21) 2,6-Dinitrotoluene 18.'07 165 134359 2.39 ug/L 72 22) Acenaphthylene 17.86 152 1155361 3.29 ug/L 98 2 3) Acenaphthene 18.42 153 825089 3.30 ug/L 97 24) 2,4-Dinitrotoluene 19.19 165 165978 2.26 ug/L 86 25) Diethylphthalate 20.00 149 985447 3.57 ug/L 97 26) 4-Chlorophenyl-phenylether 20.03 204 415177 3.58 ug/L 84 2 7) Fluorene 19.91 166 979623 3.44 ug/L 96 28) Azobenzene/1,2-Diphenylhyd 20.46 77 1055924 3.07 ug/L 84 30) N-nitrosodiphenylamine 20.43 169 540140 3.05 ug/L 99 31) 4-Bromophenyl-phenylether 21.44 248 246259 3.39 ug/L 89 32) Hexachlorobenzene 21.78 284 248719 3.24 ug/L 95 3 3) Phenanthrene 22.70 178 1473694 3.83 ug/L 98 3 4) Anthracene 22.83 178 1340383 3.59 ug/L 99 (#) = qualifier out of range (m) = manual integration 0204RB.D SCAN508.M Thu Feb 07 08:53:56 2002 Page 1

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