GCMS analysis results for sample AE00110, Feb 2002

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Data File : C:\MSDCHEM\l\5973N\02FEB04\0204C40.D Vial: 2 . Acq On : 4 Feb 2002 9:30 am Operator: Sample : cal 40 Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Feb 05 08:28:39 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCANS08

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.73 152 2067533 20.00 ug/L 0.01 10) Naphthalene-d8 13.22 136 9038294. 20.00 ug/L 0.00 17) Acenaphthene-diO 18.36 164 4890860- 20.00 ug/L 0.01 29) Phenanthrene-diO 22.67 188 8892120 20.00 ug/L 0.00 38) Chrysene-dl2 30.53 240 6985077 20.00 ug/L 0.02 44) Perylene-dl2 34.45 264 5177732 20.00 ug/L 0.03 System Monitoring Compounds 37) 2,4-DDD 27.59 235 63789 0.45 ug/L -0.14 Spiked Amount 5.000 Recovery = 9.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 4.00 74 3750664 42.57 ug/L 55 3) bis(2-Chloroethyl)ether 9.29 93 4258253 32.36 ug/L 83 4) 1,3-Dichlorobenzene 9.63 146 5323716 34.32 ug/L 97 5) 1,4-Dichlorobenzene 9.78 146 5158112 33.11 ug/L 99 6) 1,2-Dichlorobenzene 10.26 146 4254290 (30.76 ug/L 99 7) 2,2'-oxybi s (1-Chloropropa 10.69 45 7430231 31.07ug/L 96 8) n-Nitroso-di-n-propylamine 11.10 70 3572125 32.74 ug/L 85 9) Hexachloroethane 11.05 117 1902364 34.11 ug/L 95 11) Nitrobenzene 11.40 77 5701503 33.78 ug/L 86 12) 1sophorone 12.07 82 11416304 37.50 ug/L 94 13) bis(2-Chloroethoxy)methane 12.82 93 7068995 39.06 ug/L 92 14) 1,2,4-Trichlorobenzene 13.14 180 3978788 33.76 ug/L 98 15) Naphthalene 13.28 128 14791031 34.16 ug/L 99 16) Hexachlorobutadiene 13.85 225 1941419 (30.98 ug/L 99 18) Hexachlorocyclopentadiene 15.97 237 1490916 34.11 ug/L 98 19) 2-Chloronaphthalene 16.69 162 8906895 32.98 ug/L 97 20) Dimethylphthalate 17.94 163 10810230 33.47 ug/L 96 21) 2,6-Dinitrotoluene 18.11 165 2625317 41.67 ug/L 84 22) Acenaphthylene 17.90 152 13768167 34.96 ug/L 99 23) Ac enapht hene 18.47 153 8242049 (29.38 ug/L 99 24) 2,4-Dinitrotoluene 19.24 165 3900743 47.28 ug/L 97 25) Diethylphthalate 20.07 149 9081139 (29. 34 ug/L 99 26) 4-Chlorophenyl-phenylether 20.05 204 3820851 <29.37 ug/L 96 27) Fluorene 19.95 166 10999801 34.47 ug/L 99 2 8) Azobenzene/ 1,2-Diphenylhyd 20.52 77 12499725 32.39 ug/L 88 30) N-nitrosodiphenylamine 20.50 169 6160295 27.31 ug/L 99 31) 4-Bromophenyl-phenylether 21.47 248 2923609 31.59 ug/L 95 32) Hexachlorobenzene 21.81 284 3074714 31.44ug/L 99 3 3) Phenanthrene 22.75 178 15865044 32.38 ug/L 99 34) Anthracene 22.89 178 15466487 32.54 ug/L 99 (#) = qualifier out of range (m) = manual integration 0204C40.D SCAN508.M Tue Feb 05 08:28:40 2002 Page 1

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