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GCMS blank analysis results for sample AE08958, April-May 2002

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank analysis for sample AE08958 listing chemical compounds with results below detection limits.

NYC-WTC_000049522–000049534

Folder label: “GCMS X 4/16/02 A 4/24/02

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Scanned page image, NYC-WTC_000049532
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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020424\0416LB.D Vial: 3 Acq On : 24 Apr 2002 11:44 am Operator: Nefliu Sample : 04/16 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Chrysene-dl2 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.39 0.72 ug/1 2219070 Phenanthrene-dl 0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Chrysene-dl2 240 C18D12 001719-03-5 70 2 Alizarin 240 C14H804 000072-48-0 38* 3 2-Benzothiazolamine, N-(phenylme. . . 240 C14H12N2S 021816-82-0 37 4 [1,1'-Biphenyl]-4,4r-diamine, 3,... 240 C16H20N2 054827-17-7 27 Abundance Scan 4818 (31.388 min): 0416LB.D (-4809) (-) m/z 240.20 100.00% 240

5000 106 ■i* 1rr। . . । । .। . . . . । , 118 31.00 31.20 31.40 31.60 31.80

D 52 78 90 ,1 || 130 156 170 194 209 222 .. —P— m/z 241.20 42.76% niz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #91381: Chrysene-d 12 24 0

5000 31.00 31.20 31.40 31.60 31.80 m/z 236.20 38.64% JL _A 28 42 54 66 78 92 196 37° 132 156 170 182194 212 228 । i i i i [-i ■ ri । i-rrffi i'I i |"lli i-r'| i i । i । i i i l | rri ■ [ i i rr| 1’li |-i 1T miz-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #127394: Alizarin 240

31.00 31.20 31.40 31.60 31.80

_A 5000 m/z 106.10 23.80% 212 184

miz-> +27,39/51.52.7.%, 20 40 60 80 195.71155166 100 120 140 160 ; , 1.195 180 200 . 223 220 240 Abundance #91297:2-Benzothiazolamine, N-(phenylmethy!)- 24 0 31.00 31.20 31.40 31.60 31.80 m/z 239.10 20.97% 91 5000 162

106 147 39 50 65 77 ' 119 133 j ,177 206 225 I ' 1 1 1 1 1 • ‘ ' I ‘ 1 r r|- i i 'I N " . .'I'I , , j j, l . . J1', m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 31.00 31.20 31.40 31.60 31.80

0416LB.D SCAN020424.M Thu May 02 14:37:25 2002 Page 8

NYC-WTC_000049532

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NYC-WTC_000049532Source: NYC Law Department, mirrored locally

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