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GCMS blank results for sample AE00842, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.

NYC-WTC_000052233–000052250

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052249
OCR text

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB07\0111BA.D Vial: 1 Acq On : 7 Feb 2002 11:02 am Operator: Sample : lab blank 1/lla Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************** * * * ******* * * * Peak Number 12 [1,1'-Biphenyl]-4,4'-diamin... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 26.84 0.09 ug/L 52323 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 [1,1'-Biphenyl]-4,4'-diamine 184 (CA... C12H12N2 000092-87-5 9 2 Benzidine 184 C12H12N2 000092-87-5 9 3 Benzene, (4,5,5-trimethyl-1,3-cy... 184 C14H16 033930-85-7 9 4 [1,1'-Biphenyl]-4,4'-diamine (CA... 184 C12H12N2 000092-87-5 9 Abundance Scan 2055 (26.835 min): 0111 BA.D (-) m/z 184.10 100.00% 184 _...............................

5000

92 44 26.40 26.60 26.80 27.00 27.20 01 1111>>।111 * 111111' i'1 ■' 11 ■111 ’'1' i ■'111 TF m/z 185.10 28.00% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #93051: [1,1‘-Biphenyl]-4,4‘-diamine (CAS) $$ Benzidine $$... 184

5000 ' ‘I’’ 26.40 26.60 26.80 27.00 27.20 92 m/z 92.00 20.88%

n/z-> 0- TITIIIPTTTTTF 40 50 60 70 78

80 103 117 T*PITTTTTTTTTTT 130 139 90 100 110 120 130 140 150 160 170 180 190 156 167 II— Abundance #93050: Benzidine 184

26.40 26,60 26.80 27.00 27.20 5000 m/z 183.10 10.68%

78 92 V 103 117 130 139 156 167 0- IPTTPTTTT ‘Ii -TPmmP ——— iz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #93477: Benzene, (4,5,5-trimethyl-1,3-cyclopentadien-1-yl)- T—nO/nnT 1 1 1'' ' I ’ 1 184 26.40 26.60 26.80 27.00 27.20 169 m/z 44.05 6.38%

5000 154 I HMH ' M yw A ILL 141 128

0 " I'1 " 111 — TT—rr ' i'' ■ i1 ''11'1 ■' i ' ■' ■ i ■' ■ ■ i1' ■ ■ r m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 26.40 26.60 26.80 27.00 27.20

0111BA.D HP020702.M Thu Feb 21 09:58:25 2002 Page 14

NYC-WTC_000052249

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NYC-WTC_000052249Source: NYC Law Department, mirrored locally

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