GCMS blank analysis results for sample AE00110, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB04\0204BB .D Vial: 1 Acq On : 4 Feb 2002 10:58 am Operator: Sample : lab blank l/4b Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Biphenylene (CAS) $$ Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 17.86 0.06 ug/L 36658 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW Mol Form , CAS# Qual

1 Biphenylene (CAS) $$ 1,1'-Biphen... 152 C12H8 000259-79-0 86 2 Biphenylene (CAS) $$ 1,1’-Biphen... 152 C12H8 000259-79-0 83 Acenanhthak’ansyi ylene (CAS) $$ Acenapht... 152 C12H8 000208-96-8 83 4 Acenaphthylene (CAS) $$ Acenapht... 152 C12H8 000208-96-8 83 dance Scan 1269 (17.862 min): 0204BB.D (-) m/z 152.10 100.00% 152

5000

Of 49 7684 17.60 17.80 18.00 18.20 m/z 153.10 15.84% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #50548: Biphenylene (CAS) $$ 1,1-Biphenylene (CAS) $$ Dip... 152

5000 17.60 17.80 18.00 18.20 m/z 151.00 15.77%

miz-> 76 87 98 O+ TTm—mmmter 40 50 60 70 80 90 100 126 110 120 130 140 150 . Ila 160 Abundance #50549: Biphenylene (CAS) $$ 1,1 '-Biphenylene (CAS) $$ Dip... 152 1 11 1 r r 1 i'» ■ • i ' 1 1 1 I'1 17.60 17.80 18.00 18.20 5000 m/z 150.10 15.48%

76 ii 87 98 126 140 11 Of miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #50557: Acenaphthylene (CAS) $$ Acenaphthalene $$ ACENAPHT... ■ ‘ i ■ ■ ■ ■ i ■ ■ i ■ ■ ' ■ i 1 ■ 152 17.60 17.80 18.00 18.20 m/z 76.00 14.78% 5000

63 76 126 O T0d——.’m—Ime!— , tno*uu 87 98 “wTuvtpr BIT m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 17.60 17.80 18.00 18.20

I204BB.D SCAN508.M Tue Feb 05 09:47:46 2002 Page 10

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