GCMS sample analysis report AE08482, May 7 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020419\0410REF2.D Vial: 8 Acq On : 19 Apr 2002 3:00 pm Operator: Nefliu Sample : 04/10 ref Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 19 15:47:34 2002 Quant Results File: SCAN020418 .RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Fri Apr 19 13:40:58 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 10377103 40.00 ug/1 -0.05 10) Naphthalene-d8 16.54 136 40199798 40.00 ug/1 -0.06 17) Acenaphthene-dl0 24.47 164 21743526 40.00 ug/1 -0.06 31) Phenanthrene-diO 31.72 188 32249136 40.00 ug/1 -0.05 39) Chrysene-dl2 39.94 240 24194907 40.00 ug/1 -0.07 45) Perylene-dl2 43.16 264 16859684 40.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 27.54 207 1005179 7.44 ug/1 -0.07 Spiked Amount 10.000 Recovery = 74.40% Target Compounds Qvalue 2) N-nitrosodimethylamine 4.00 74 1291593m 7.74 ug/1 3) bis(2-Chloroethyl)ether 10.66 93 4919526 14.34 ug/1 99 4) 1.3-Dichlorbenzene 11.12 146 4597133 12.53 ug/1 99 5) 1,4-Dichlorobenzene 11.44 146 4789340 12.03 ug/1 98 6) 1,2-Dichlorobenzene 11.96 146 4794712 13.72 ug/1 99 7) 2,2'oxybis(1-Chioropropane 12.79 45 7460190m 15.45 ug/1 8) N-Nitroso-di-n-propylamine 13.26 43 2628146 14.61 ug/1 98 9) Hexachloroethane 13.26 119 1212933 8.89 ug/1 91 11) Nitrobenzene 13.67 77 3627931 12.28 ug/1 98 12) 1sophorone 14.79 82 7312636 12.57 ug/1 97 13) bis(2-Chloroethoxy) methan 16.03 93 6100232 14.89 ug/1 96 14) 1,2,4-Trichlorobenzene 16.39 180 3851660 13.48 ug/1 99 15) Naphthalene 16.62 128 14886653 15.53 ug/1 98 16) Hexachlorobutadiene 17.40 225 1298265 10.08 ug/1 96 18) Hexachiorocyclopentadiene 20.59 237 170506 1.70 ug/1 87 19) 2-Chloronaphthalene 21.93 162 9122117 17.18 ug/1 97 2 0) Acenaphthylene 23.75 152 13339724 13.73 ug/1 97 21) Dimethyl phthalate 23.85 163 10614964 16.32 ug/1 99 22) 2,6-Dinitrotoluene 23.96 77 329623 10.90 ug/1 # 87 23) Acenaphthene 24.60 153 8906425 16.20 ug/1 98 24) 2,4-Dinitrotoluene 25.74 165 1268774 10.61 ug/1 100 25) Fluorene 27.01 166 10780798 16.96 ug/1 96 26) Diethyl phthalate 27.23 149 9895211 17.03 ug/1 99 27) 4-Chlorophenyl-phenylether 27.35 204 4594441 16.06 ug/1 99 29) N-Nitrosodiphenylamine 27.95 168 2276701 11.19 ug/1 # 88 3 0) Azobenzene 28.03 77 9177609 13.54 ug/1 93 32) Hexachlorobenzene 29.60 284 2982289 18.10 ug/1 97 33) 4-Bromophenyl-phenylether 29.71 248 2560817 16.36 ug/1 88 34) Phenanthrene 31.82 178 15198074m 16.89 ug/1 35) Anthracene 32.05 178 13103755 14.15 ug/1 98 (#) = qualifier out of range (m) = manual integration 0410REF2.D SCAN020418.M Mon Apr 22 15:34:29 2002 Page 1

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