GCMS reference results, sample AE07767, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020404\0403REF2.D Vial: 18 Acq On 4 Apr 2002 10:47 pm Operator: Nefliu Sample 04/03 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 05 14:20:03 2002 Quant Results File: SCAN020403.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Fri Apr 05 14:03:06 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 10.66 152 2380626 20.00 ug/1 0.00 10) Naphthalene-d8 15.77 136 8741487 20.00 ug/1 0.00 17) Acenaphthene-dlO 23.66 164 4999535 20.00 ug/1 -0.01 31) Phenanthrene-dlO 30.89 188 8093990 20.00 ug/1 0.00 39) Chrysene-dl2 39.10 240 6829041 20.00 ug/1 -0.01 45) Perylene-dl2 42.30 264 3611976 20.00 ug/1 -0.01

System Monitoring Compounds 2 8) TCMX 26.73 207 221843 4.53 ug/1 0.00 Spiked Amount 4.000 Recovery = 113.25%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.67 74 307365m 4.66 ug/1 3) bis(2-Chloroethyl)ether 9.94 93 1116548 9.00 ug/1 97 4) 1.3-Dichlorbenzene 10.40 146 1314600 7.70 ug/1 98 5) 1,4-Dichlorobenzene 10.72 146 1354013 7.82 ug/1 99 6) 1,2-Dichlorobenzene 11.23 146 1289944 7.89 ug/1 99 7) 2,2'oxybis(1-Chloropropane 12.04 45 935409 11.30 ug/1 97 8) N-Nitroso-di-n-propylamine 12.50 43 680357 9.82 ug/1 99 9) Hexachloroethane 12.51 119 420049 7.80 ug/1 100 11) Nitrobenzene 12.92 77 978515 7.97 ug/1 98 12) Isophorone 14.02 82 1905469 8.43 ug/1 97 13) bis(2-Chloroethoxy) methan 15.25 93 1399374 9.43 ug/1 99 14) 1,2,4-Trichlorobenzene 15.61 180 1123198 8.12 ug/1 99 15) Naphthalene 15.85 128 3778844 9.02 ug/1 99 16) Hexachlorobutadiene 16.62 225 601733 7.75 ug/1 98 18) Hexachlorocyclopentadiene 19.80 237 69321 1.56 ug/1 93 19) 2-Chloronaphthalene 21.13 162 2357336 8.60 ug/1 100 20) Acenaphthylene 22.95 152 3362662 8.78 ug/1 100 21) Dimethyl phthalate 23.04 163 2908190 9.79 ug/1 100 22) 2,6-Dinitrotoluene 23.15 77 112842m 9.98 ug/1 23) Acenaphthene 23.79 153 2517205 9.10 ug/1 99 24) 2,4-Dinitrotoluene 24.92 165 441593 9.59 ug/1 99 25) Fluorene 26.20 166 2838452 9.02 ug/1 100 26) Diethyl phthalate 26.41 149 2808352 9.83 ug/1 100 27) 4-Chlorophenyl-phenylether 26.53 204 1364060 8.94 ug/1 97 29) N-Nitrosodiphenylamine 27.13 168 965479 8.28 ug/1 98 30) Azobenzene 27.21 77 2590660 9.38 ug/1 100 32) Hexachlorobenzene 28.77 284 955307 8.48 ug/1 97 33) 4-Bromophenyl-phenylether 28.89 248 802496 8.73 ug/1 98 34) Phenanthrene 30.99 178 4287132 9.61 ug/1 99 35) Anthracene 31.22 178 3775224 8.66 ug/1 100

(#) = qualifier out of range (m) = manual integration 0403REF2.D SCAN020403.M Fri Apr 05 14:20:50 2002 Page 1

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