Laboratory blank analysis results confirming absence of contamination in GCMS testing for volatile organic compounds.
NYC-WTC_000048602–000048610Folder label: “GCMS X 4/10/02 A 4/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020419\0410LB.D Vial: 4 Acq On : 19 Apr 2002 11:03 am Operator: Nefliu Sample : 04/10 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C: \DATABASE\ni s 198.1 ********************************************************************* Peak Number 2 2-Imidazolidinone, 1-methox... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.30 ug/1 655977 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Imidazolidinone, 1-methoxy-3-p. . . 192 C10H12N2O2 052420-43-6 40 2 2-Propenal, 3-(3,4-dimethoxyphen. . . 192 C11H1203 004497-40-9 39 3 9H-Fluorene, 9-ethylidene- 192 C15H12 007151-64-6 9 4 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 9 Abundance Scan 4768 (31.094 min): 0410LB.D (-4761) (-) m/z 192.05 100.00% 1912
40 5000
96 . ..... 7A......... 30.80 31.00 31.20 31.40
n/z—> 60 70 82 | 122 146 160 JU- I .. I. I.. |, i I. I! I , I I | I I I I | I ! 1 I | I I n | I I I'l | I I I I | I ′ | I I I I'l I I ! I | ! I I I | I I 1111
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 40.10 57.31% Abundance #80907:2-Imidazolidinone, 1-methoxy-3-phenyl- 106 192
77 119 162 5000 42 30.80 31.00 31.20 31.40 56 91 m/z 96.20 17.87% 28 64 n/z—> m mm ljunipualapu I.... 134 T 1111 " " 111" I I_____________ ‘• * I • * ‘ ‘ I “ * ’ I r” ’ Ir 20 30 40 a) 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxypheny!)- 19/2 161 30.80 31.00 31.20 31.40 5000 m/z 191.00 16.99% A 77 91 . 121 149 177 103 | 138 | ( 52 64 1 ।| i 1. . ′ . . । .'I I . ।. . JI । . ■ i rre...... | I'l 11‘...... i 1_ | I ..re .................... i | 1′14 r_ 111 11 |1ii 111 > I'l . rpt i i i rro > | I I i‘i । I I I I MI i 11 i 1111 /z—> 20 30 40 50 60 70 80 100 110 120 130 140 1S) 160 170 180 190 200 -............... Abundance #81028:9H-Fluorene, 9-ethylidene- 1112 30.80 31.00 31.20 31.40 m/z 193.10 14.23%
5000 165
83 99 - 41 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 ISO' 160 170 180 190 200 30.80 31.00 31.20 31.40
0410LB.D SCAN020418.M Thu May 02 11:39:51 2002 Page 4
NYC-WTC_000048608
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NYC-WTC_000048085
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048169
Laboratory report documenting GCMS analysis of sample AE08426 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048207
Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048635
GC/MS analysis report for sample AE08486 conducted May 7, 2002, detecting unknown compounds and surrogate standard 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048195
Laboratory report documenting GCMS analysis of sample AE08428 conducted on May 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047302
Laboratory data sheet recording method 50 analysis parameters including drip rate and pH measurements from April 2002.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046117
Laboratory report showing GCMS blank results for volatile organic compounds from sample AE10068 dated May 7-13, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024427
Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024534
Laboratory report showing blank test results for GCMS analysis of sample AE11282 conducted between May 13 and May 16, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024748
Reference document describing Method 509 procedures for laboratory analysis, dated February 14, 1992.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025499
Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022495
Technical log detailing gas chromatography mass spectrometry method parameters and calibration settings from May 2002.
1 shared topics · similarity 0.991
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NYC-WTC_000048598
Department of Environmental Protection GCMS analysis record containing a redacted name dated April 10-20, 2002.
Filed in the same folder
NYC-WTC_000048599
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
Filed in the same folder
NYC-WTC_000048611
Laboratory calibration data for GCMS analysis of volatile organic compounds including nitrosamines and chlorobenzenes.
Filed in the same folder
NYC-WTC_000048615
Reference standard analysis results for volatile organic compounds used to verify GCMS instrument performance.
Filed in the same folder
NYC-WTC_000048620
Gas chromatography-mass spectrometry results for sample AE08482 including surrogate recovery data.
Filed in the same folder