GCMS calibration scan data, Sample 5844, April 4 2002

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Data File C:\HPCHEM\1\DATA\APR0 3 022\5750.D Vial: 17 Acq On 4 Apr 2002 11:27 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclohexene, 1-methoxy- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

21.08 0.54 ug/1 33805 Acenaphthene-dl0 21.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexene, 1-methoxy- 112 C7H120 000931-57-7 12 2 Cyclohexanamine, N,N-dimethyl- 127 C8H17N 000098-94-2 10 3 2-Pyrrolidinecarboxamide, 5-oxo-, ( 128 C5H8N202 016395-57-6 10 4 2,3,4,5-Tetrahydropyridazine 84 C4H8N2 000694-06-4 10 Abundance Scan 1746 (21.078 min): 5750.D (-) m/z 55.00 100.00% 55 A

84 5000 41 . 100 111 129 4 20.80 21.00 21.20 21.40 . ..... I , -H TIT I— — ' r '1'i 1 1 1 ‘I 1 11 11 1 1 1 'i 30 40 50 60 70 80 71 1 > 11111 j 11111111 156 m/z 83.95 60.04% mlz—> 20 90 100 110 120 130 140 150 160 Abundance #63985: Cyclohexene, 1 -methoxy- N 84 112

5000 97 uE94AAA/YW444 20.80 21.00 21.20 21.40 54 m/z 129.00 33.69% 27 69 45 1 i ' ■ 1 1 i ' ......... . ,I L ■ ' i ' ' '1 i1 1 ' j' I I I I f I I I I I I I I

mz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #64992: Cyclohexanamine, N,N-dimethyl- 84

20.80 21.00 21.20 21.40 5000 m/ z 41.05 33.27%

42 /I 127 1I 58 IPPPPI J i I | r i 98 i I | i r i i [ i i i i | i i I I I-1 i i i i | i i i i | i i i i J“1 T

m/z-> Abundance 20 30 40 50 60 70 80 90 #4852: 2-Pyrrolidinecarboxamide, 5-oxo-, (S)- 84 100 110 120 130 140 150 160 .. . 1.. 20.80 21.00 21.20 21.40 m/z 111.00 30.00% 55 44 5000

66 128

n/z—> JU ‘T‘171 । । । । । । । । 11 1 i 1 20 30 40 50 I........................ 90 100 110 120 130 140 150 160 60 70 80 ‘"70110—U11TTTT1nt I j i I i r | i i i 1 . | I I ■ ■ । ■ ■ ■ - । ■ i । । । 1 । । - 20.80 21.00 21.20 21.40

5750.D GCMS0408.M Tue Apr 16 08:15:54 2002 Page 3

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