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GCMS method file details, sample AE07767, April 2002

Machine-extracted title · confidence 100%

Technical documentation listing GC/MS method parameters and internal standard data for analysis performed in early April 2002.

NYC-WTC_000047449–000047451

Folder label: “GCMS X 4/3/02 A 4/5/02

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Scanned page image, NYC-WTC_000047450
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020404\0403REFl.D Vial: 17 Acq On 4 Apr 2002 9:52 pm Operator: Nefliu Sample 04/03 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 05 14:19:07 2002 Quant Results File: SCAN020403.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Fri Apr 05 14:03:06 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Di-n-butylphthalate 33.98 149 3256990 7.65 ug/1 99 37) Fluoranthene 35.22 202 3367636 7.39 ug/1 96 40) Pyrene 35.83 202 3562374 8.67 ug/1 97 41) Buthylbenzylphthalate 38.09 149 937872 6.23 ug/1 94 42) Benz(a)anthracene 39.08 228 2803011 7.80 ug/1 100 43) Chrysene 39.15 228 2823989 8.41 ug/1 99 44) Bis(2-ethylhexyl)phthalate 39.68 149 1102475 5.77 ug/1 96 46) Di-n-Octyl phthalate 41.19 149 974997 5.57 ug/1 93 47) Benzo(b)fluoranthene 41.52 252 1939379 7.65 ug/1 97 48) Benzo(k)fluoranthene 41.58 252 2268417 8.23 ug/1 96 49) Benzo(a)pyrene 42.17 252 1336455m 5.76 ug/1 50) Indeno(1,2,3-cd)pyrene 44.35 276 653680 6.84 ug/1 95 51) Dibenz(a,h)anthracene 44.44 278 895414 5.06 ug/1 94 52) Benzo(ghi)perylene 44.89 276 1003153 5.25 ug/1 97

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0403REF1.D SCAN020403.M Fri Apr 05 14:19:50 2002 Page 2

NYC-WTC_000047450

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NYC-WTC_000047450Source: NYC Law Department, mirrored locally

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