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GCMS reference standard results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Calibration data report for GCMS analysis of volatile organic compounds performed on April 2-3, 2002.

NYC-WTC_000047181–000047185

Folder label: “GCMS X 4/2/02 A 4/3/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020403\0402REFl.D Vial: 11 Acq On 3 Apr 2002 6:17 pm Operator: Nefliu Sample 04/02 ref Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 04 08:40:10 2002 Quant Results File: SCAN020403.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Thu Apr 04 08:40:00 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Di-n-butylphthalate 33.98 149 4541642 8.05 ug/1 100 37) Fluoranthene 35.23 202 5181025 8.57 ug/1 98 40) Pyrene 35.83 202 5493427 8.68 ug/1 99 41) Buthylbenzylphthalate 38.10 149 1622905 6.99 ug/1 98 42) Benz(a)anthracene 39.08 228 4876832 8.80 ug/1 100 43) Chrysene 39.16 228 4921787 9.50 ug/1 99 44) Bis(2-ethylhexyl)phthalate 39.68 149 2089238 7.09 ug/1 97 46) Di-n-Octyl phthalate 41.19 149 2556825 6.74 ug/1 97 47) Benzo(b)fluoranthene 41.53 252 4173827 8.60 ug/1 98 48) Benzo(k)fluoranthene 41.59 252 4404176 8.35 ug/1 98 49) Benzo(a)pyrene 42.18 252 2829862 6.37 ug/1 97 50) Indeno(1,2,3-cd)pyrene 44.35 276 2192937 8.95 ug/1 98 51) Dibenz(a,h)anthracene 44.45 278 2714932 8.02 ug/1 97 52) Benzo(ghi)perylene 44.89 276 2781290 7.61 ug/1 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0402REF1.D SCAN020403.M Thu Apr 04 08:40:59 2002 Page 2

NYC-WTC_000047184

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NYC-WTC_000047184Source: NYC Law Department, mirrored locally

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