2
z Quantitation Report (QT Reviewed) -
K o
o
2 Data File
Acq On
C:\MSDCHEM\l\DATA\020403\0402REFl.D
3 Apr 2002 6:17 pm
Vial : 11
Operator: Nefliu
co
—
o "0
I Sample 04/02 ref Inst : Instrumen C
o O
o
o Mise Multiplr: 1.00 o'
o
MS Integration Params: EVENTS.E "0
o
00
Quant Time: Apr 4 8:40 2002 Quant Results File: SCAN020403.RES 0
CH
U
Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) o
Q
C
Title : Method 508 GC/MS Scan 3
Last Update : Thu Apr 04 08:40:00 2002
Response via : Initial Calibration
Abundance TIC: 0402REF1.D
1800000
2m
9
1600000 s
H
1400000 i' N
zs
3 &
1200000 o
$
8
e
z
2
&
1000000 iS 2o
16
£
C
€
c
2
2 o
a
I §
z 12
()
800000
3
Il
§ & O
g u o
I d 1 P P Ctj
it
I
0
2c 2 Pp
S0p
o
12 I I2 l ?
I
O
6o
g
600000 OC-
8& fi S8
lal it m
Mill @.S 7
2 2
2 o
I £
5
2 &4
C
c
a
88
f
I
287 3 5
400000
gka 22
Q
If 3
8
3
8o
g
N
s 11 I 68
C
200000
3e 11 N
8
9
No
2
t—
s
X o
8
o
3
5
I
0- _____ UUUL I I I I I I “I I I I I I I I
1 1 । 1 ■ 1 1 । 1
________ ___ I_
i i | । i i । | t f i r | i i i < | ।
I __ —.... —
1 I 1 1 1 ' I '
rime-s 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00
Gas chromatography-mass spectrometry analysis of sample AE07627 conducted April 9, 2002, detecting unknown compounds and 2,4-DDD surrogate at 94% recovery.