GCMS method file details, sample AE07767, April 2002

2 Quantitation Report (QT Reviewed) z - K o o 2 Data File Acq On C:\MSDCHEM\1\DATA\020404\0403REF1.D Vial: 17 CD — o 4 Apr 2002 9:52 pm Operator: Nefliu "0 1 O O Sample 04/03 ref Inst : Instrumen C O Si Mise Multiplr: 1.00 o' L MS Integration Params: EVENTS.E "0 o C Quant Time: Apr 5 14:19 2002 Quant Results File: SCAN020403.RES — 0 o o Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Q Title : Method 508 GC/MS Scan C 3 Last Update : Fri Apr 05 14:03:06 2002 CD

Response via : Initial Calibration Abundance TIC: 0403REF1.D

1200000 2o s € 1100000 % ad ¥ a । t> 1000000 I5 8 900000 5 & 1 C 8 Ia o 800000 a I8 700000

600000 1i tzg c 2

2 Q. &

I 2 1 g 1 f , I s8 d i) 500000 6 ! o C £ 2 2 o2 68 i L aco I

I 2 g2» % 5 285 2 8 5 1 fg 400000 ill if §42 a W 3 ® & I c E 1 | ? ii I 8gs f2 f g

? I 2 8€ 2 e 5 300000 I 2 8 5 2 A5 of -2

t i S ao CM 2 §

200000 I 488 hg o 1 x 53 N 8 P X 8 §b o z 5 .52 CO

[l g Z o X

I ? S I c V o 100000 8

Time-> 0—. । . P-r 4.00 6.00 8.00 UU 10.00 L 12.00 14.00 16.00 18.00 I

20.00 22.00 24.00 —U 26.00 I IL 28.00 30.00 32.00 —

34.00 36.00 38.00 40.00 42.00 44.00

0403REF1.D SCAN020403.M Fri Apr 05 14:19:50 2002 Page 3