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GCMS reference standard results for volatile organics, Apr-May 2002

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Reference standard analysis results for volatile organic compounds used to verify GCMS instrument performance.

NYC-WTC_000048615–000048619

Folder label: “GCMS X 4/10/02 A 4/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020419\0410REF1.D Vial: 6 Acq On : 19 Apr 2002 1:02 pm Operator: Nefliu Sample : 04/10 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 19 14:06:14 2002 Quant Results File: SCAN020418 .RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Fri Apr 19 13:40:58 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue 36) Di-n-butylphthalate 34.81 149 19157973 16.56 ug/1 99 37) Fluoranthene 36.06 202 16399894 17.73 ug/1 84 40) Pyrene 36.66 202 17215898 17.44 ug/1 91 41) Buthylbenzylphthalate 38.93 149 7415765 14.82 ug/1 95 42) Benz(a)anthracene 39.92 228 13861693 16.96 ug/1 97 43) Chrysene 40.00 228 13404877 17.83 ug/1 97 44) Bis(2-ethylhexyl)phthalate 40.53 149 9655118 15.72 ug/1 92 46) Di-n-Octyl phthalate 42.04 149 14433173 12.71 ug/1 95 47) Benzo(b)fluoranthene 42.37 252 11920554m 15.64 ug/1 48) Benzo(k)fluoranthene 42.44 252 11914146 15.71 ug/1 88 4 9) Benzo(a)pyrene 43.02 252 8425693m 11.68 ug/1 50) Indeno(1,2,3-cd)pyrene 45.22 138 2894754 16.56 ug/1 44 51) Dibenz(a,h)anthracene 45.32 139 2566429 19.60 ug/1 78 52) Benzo(ghi)perylene 45.78 276 8044192 19.78 ug/1 84

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0410REF1.D SCAN020418.M Mon Apr 22 15:33:20 2002 Page 2

NYC-WTC_000048618

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NYC-WTC_000048618Source: NYC Law Department, mirrored locally

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