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GCMS calibration scan data for volatile organics, April 2002

Machine-extracted title · confidence 100%

Instrument scan data for GCMS calibration using deuterated standards on April 19, 2002.

NYC-WTC_000048103–000048105

Folder label: “GCMS X 4/9/02 A 4/19/02

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NYC 9/11 Public Portal Document

/ Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020419\0409REFl.D Vial: 5 Acq On : 19 Apr 2002 12:03 pm Operator: Nefliu Sample : 04/09 ref Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 19 13:41:24 2002 Quant Results File: SCAN020418.RE

Quant Method : C: \MSDCHEM\1\METHODS\SCAN020418 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Fri Apr 19 13:40:58 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Di-n-butylphthalate 34.81 149 16755896 16.21 ug/1 98 37) Fluoranthene 36.06 202 14318859 17.33 ug/1 84 40) Pyrene 36.66 202 15109906 16.69 ug/1 91 41) Buthylbenzylphthalate 38.93 149 6394597 13.93 ug/1 93 42) Benz(a)anthracene 39.92 228 12376145 16.51 ug/1 96 43) Chrysene 40.00 228 11889124 17.24 ug/1 97 44) Bis (2-ethylhexyl) phthalate 40.53 149 8522094 15.13 ug/1 93 46) Di-n-Octyl phthalate 42.04 149 12818400 12.32 ug/1 95 47) Benzo(b)fluoranthene 42.37 252 10528155m 15.07 ug/1 48) Benzo(k)fluoranthene 42.44 252 10645296 15.33 ug/1 90 49) Benzo(a)pyrene 43.02 252 8004550m 12.11 ug/1 50) Indeno(1,2,3-cd)pyrene 45.22 138 2593839 16.19 ug/1 # 43 51) Dibenz(a,h)anthracene 45.32 139 2293289 19.12 ug/1 # 80 52) Benzo(ghi)perylene 45.77 276 7203801 19.34 ug/1 84

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0409REF1.D SCANO20418.M Fri Apr 26 15:05:45 2002 Page 2

NYC-WTC_000048104

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NYC-WTC_000048104Source: NYC Law Department, mirrored locally

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