GCMS reference analysis results for sample AE07311, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR0302\CAL40.D Vial: 2 Acq On 3 Apr 2002 12:38 pm C Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 8 10:57 2002 Quant Results File: GCMS0403.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Mon Apr 08 10:55:57 2002 Response via Initial Calibration DataAcq Meth GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 581139 20.00 ug/1 -0.01 10) Naphthalene-d8 15.89 136 2171821 20.00 ug/1 -0.01 17) Acenaphthene-diO 21.20 164 1231509 20.00 ug/1 0.00 30) Phenanthrene-diO 25.64 188 1867023 20.00 ug/1 -0.01 39) Chrysene-dl2 33.70 240 1047841 20.00 ug/1 -0.01 45) Perylene-dl2 37.94 264 553946 20.00 ug/1 -0.01

System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds 2) N-nitroso-dimethyl amine 5.89 74 658093 2% 52 41.88 ug/1 Qvalue 100 3) bis(2-Chloroethyl)ether 11.66 93 1021364 40.06 ug/1 98 4) 1,3-Dichlorobenzene 12.15 146 1136115 41.76 ug/1 99 5) 1,4-Dichlorobenzene 12.30 146 1151883 42.10 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 1063156 41.55 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.13 45 1378437 40.43 ug/1 99 8) N-Nitroso-di-n-propylamine 13.53 70 674796 41.83 ug/1 99 9) Hexachloroethane 13.66 117 414886 41.70 ug/1 96 11) Nitrobenzene 13.95 77 1004796 41.01 ug/1 98 12) Isophorone 14.59 82 1882732 41.25 ug/1 99 13) bis(2-Chloroethoxy)methane 15.27 93 1247879 41.09 ug/1 100 14) 1,2,4-Trichlorobenzene 15.77 180 938214 41.46 ug/1 100 15) Naphthalene 15.95 128 2873886 41.56 ug/1 100 16) Hexachlorobutadiene 16.49 225 482661 41.93 ug/1 99 18) Hexachlorocyclopentadiene 18.68 237 339545 42.85 ug/1 99 19) 2-Chloronaphthalene 19.46 162 1789885 41.78 ug/1 99 20) Dimethylphthalate 20.55 163 2059686 41.61 ug/1 100 21) 2,6-Dinitrotoluene 20.77 165 491457 42.09 ug/1 96 22) Acenaphthylene 20.72 152 2522139 42.25 ug/1 100 23) Acenaphthene 21.29 153 1775026 41.83 ug/1 99 24) 2,4-Dinitrotoluene 21.93 165 638851 42.72 ug/1 99 25) Diethylphthalate 22.69 149 1946451 41.83 ug/1 99 26) 4-Chlorophenyl-phenylether 22.83 204 906417 42.05 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0403.M Mon Apr 08 10:58:54 2002 Page 1

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