GCMS calibration results for sample AE08012, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\1\DATA\APR1102\CAL25 . D Vial: 4 Acq On 11 Apr 2002 12:26 pm Operator: Sample 5 Inst Multiplr: : 209 1.00 Mise MS Integration Params: GOOFY.P Quant Time: Apr 16 11:37 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 11:36:35 2002 Response via : Initial Calibration DataAcq Meth : GCMS0408

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.24 152 603914 20.00 ug/1 0.00 10) Naphthalene-d8 15.88 136 2248973 20.00 ug/1 0.00 17) Acenaphthene-diO 21.17 164 1290407 20.00 ug/1 0.00 30) Phenanthrene-diO 25.62 188 1947931 20.00 ug/1 0.00 39) Chrysene-dl2 33.68 240 1294069 20.00 ug/1 0.00 45) Perylene-dl2 37.92 264 845331 20.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery 0. 00% (6 n 1 Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.88 74 662513 50.41 ug/1 99 3) bis(2-Chloroethyl)ether 11.65 93 1013299 49.53 ug/1 98 4) 1,3-Dichlorobenzene 12.14 146 1052610 49.90 ug/1 100 5) 1,4-Dichlorobenzene 12.28 146 1058706 49.87 ug/1 98 6) 1,2-Dichlorobenzene 12.80 146 983220 49.87 ug/1 99 7) 2,21-oxybis(1-Chloropropan 13.11 45 1413071 50.00 ug/1 99 8) N-Nitroso-di-n-propylamine 13.52 70 673284 50.18 ug/1 99 9) Hexachloroethane 13.64 117 390268 50.17 ug/1 99 11) Nitrobenzene 13.93 77 983875 49.90 ug/1 99 12) Isophorone 14.57 82 1873481 50.22 ug/1 99 13) bis(2-Chloroethoxy)methane 15.25 93 1224259 50.38 ug/1 99 14) 1,2,4-Trichlorobenzene 15.76 180 856427 50.09 ug/1 100 15) Naphthalene 15.93 128 2723866 50.37 ug/1 100 16) Hexachlorobutadiene 16.47 225 427266 49.97 ug/1 99 18) Hexachlorocyclopentadiene 18.67 237 301004 52.74 ug/1 99 19) 2-Chloronaphthalene 19.44 162 1687166 49.58 ug/1 100 20) Dimethylphthalate 20.53 163 1947030 49.63 ug/1 99 21) 2,6-Dinitrotoluene 20.75 165 473056 50.43 ug/1 96 22) Acenaphthylene 20.70 152 2383874 50.07 ug/1 100 23) Acenaphthene 21.27 153 1690501 49.95 ug/1 100 24) 2,4-Dinitrotoluene 21.92 165 616881 49.96 ug/1 98 25) Diethylphthalate 22.67 149 1865188 49.56 ug/1 100 26) 4-Chlorophenyl-phenylether 22.81 204 847956 50.78 ug/1 98 27) Fluorene 22.80 166 1821676 50.83 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.28 77 1922713 48.28 ug/L 97 31) N-Nitrosodiphenylamine 23.21 168 814369 50.26 ug/1 98 32) 4-Bromophenyl-phenylether 24.28 248 472012 49.91 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS0412.M Tue Apr 16 11:44:30 2002 Page 1

NYC-WTC_000047653