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GCMS calibration results for sample AE08012, April 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS calibration data for sample AE08012 conducted on April 17, 2002, listing target compounds and concentrations.

NYC-WTC_000047652–000047655

Folder label: “GCMS X 4/4/02 A 4/12/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR110 2\CAL2 5.D Vial: 4 Acq On 11 Apr 2002 12:26 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 16 11:37 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 11:36:35 2002 Response via : Initial Calibration DataAcq Meth : GCMS0408

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.72 284 556655 49.75 ug/1 98 34) Phenanthrene 25.69 178 2543312 50.55 ug/1 100 35) Anthracene 25.83 178 2538309 51.30 ug/1 100 36) Di-n-butylphthalate 27.59 149 3203819 50.91 ug/1 100 37) Fluoranthene 29.32 202 2571065 50.81 ug/1 98 4 0) Pyrene 29.99 202 2609508 50.20 ug/1 97 41) Butylbenzylphthalate 32.12 149 1281532 50.41 ug/1 97 42) Benzo(a)anthracene 33.62 228 1824222 50.59 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.89 149 1638083 50.36 ug/1 100 44) Chrysene 33.76 228 1787189 49.98 ug/1 100 46) Di-n-Octylphthalate 35.63 149 2521609 50.49 ug/1 99 47) Benzo(b)fluoranthene 36.73 252 1578733 48.93 ug/1 99 48) Benzo(k)fluoranthene 36.81 252 1581564 50.34 ug/1 100 49) Benzo(a)pyrene 37.72 252 1347373 50.65 ug/1 99 50) Indeno(1,2,3-cd)pyrene 42.03 276 1382088 51.60 ug/1 99 51) Dibenz(a,h)anthracene 42.10 278 1057015 51.76 ug/1 100 52) Benzo(g,h,i)perylene 43.28 276 1152829 51.56 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS0412.M Tue Apr 16 11:44:32 2002 Page 2

NYC-WTC_000047654

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NYC-WTC_000047654Source: NYC Law Department, mirrored locally

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