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GCMS calibration verification data for volatile organics, Apr 2002

Machine-extracted title · confidence 100%

Calibration verification records for gas chromatography-mass spectrometry analysis of volatile organic compounds.

NYC-WTC_000043340–000043343

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR2402\CAL50.D Vial: 2 Acq On 24 Apr 2002 4:49 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 25 9:52 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.69 284 410948 54.44 ug/1 95 34) Phenanthrene 25.66 178 1695382 49.94 ug/1 99 35) Anthracene 25.79 178 1705508 51.08 ug/1 99 36) Di-n-butylphthalate 27.56 149 2085921 49.12 ug/1 100 37) Fluoranthene 29.28 202 1696977 49.70 ug/1 98 40) Pyrene 29.96 202 1719572 49.78 ug/1 96 41) Butylbenzylphthalate 32.09 149 761988 45.11 ug/1 96 42) Benzo(a)anthracene 33.60 228 1192572 49.77 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 914722 42.32 ug/1 99 44) Chrysene 33.72 228 1189192 50.05 ug/1 99 46) Di-n-Octylphthalate 35.61 149 1304684 42.64 ug/1 # 99 47) Benzo(b)fluoranthene 36.70 252 926564 46.88 ug/1 98 48) Benzo(k)fluoranthene 36.77 252 1079678 56.09 ug/1 98 49) Benzo(a)pyrene 37.68 252 831855 51.04 ug/1 99 50) Indeno(1,2,3-cd)pyrene 41.97 276 738068 44.98 ug/1 98 51) Dibenz(a,h)anthracene 42.04 278 574301 45.90 ug/1 98 52) Benzo(g,h,i)perylene 43.20 276 582657 42.54 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL50.D GCMS0412.M Thu Apr 25 09:56:01 2002 Page 2

NYC-WTC_000043342

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NYC-WTC_000043342Source: NYC Law Department, mirrored locally

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