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GCMS calibration results for sample AE09095, April 2002

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Laboratory report displaying GCMS calibration data for sample AE09095 conducted on April 23, 2002.

NYC-WTC_000046468–000046471

Folder label: “GCMS X 4/17/02 A 4/24/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR2302\CAL80.D Vial: 2 Acq On 23 Apr 2002 3:21 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 8:08 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.70 284 732095 85.22 ug/1 95 34) Phenanthrene 25.67 178 3058868 79.19 ug/1 100 35) Anthracene 25.81 178 3025727 79.64 ug/1 100 36) Di-n-butylphthalate 27.57 149 3700996 76.59 ug/1 100 37) Fluoranthene 29.30 202 3086263 79.43 ug/1 95 4 0) Pyrene 29.98 202 3109631 78.21 ug/1 94 41) Butylbenzylphthalate 32.10 149 1410787 72.56 ug/1 95 42) Benzo(a)anthracene 33.60 228 2196802 79.65 ug/1 100 43) Bis(2-ethylhexyl)phthalate 33.87 149 1702408 68.43 ug/1 99 44) Chrysene 33.74 228 2150614 78.63 ug/1 100 46) Di-n-Octylphthalate 35.61 149 2517865 71.93 ug/1 # 99 47) Benzo(b)fluoranthene 36.71 252 1885457 83.37 ug/1 98 48) Benzo(k)fluoranthene 36.79 252 1813475 82.34 ug/1 98 49) Benzo(a)pyrene 37.70 252 1571168 84.26 ug/1 99 50) Indeno(1,2,3-cd)pyrene 41.99 276 1434277m 76.40 ug/1 51) Dibenz(a,h)anthracene 42.07 278 1112346 77.70 ug/1 96 52) Benzo(g,h,i)perylene 43.23 276 1123079 71.66 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0412.M Wed Apr 24 11:13:21 2002 Page 2

NYC-WTC_000046470

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NYC-WTC_000046470Source: NYC Law Department, mirrored locally

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