GCMS calibration results for sample AE09095, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR2302\CAL80.D Vial: 2 Acq On 23 Apr 2002 3:21 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 8:08 2002 Quant Results File: GCMS0412.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Wed Apr 17 11:48:30 2002 Response via Initial Calibration DataAcq Meth GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.22 152 467726 20.00 ug/1 -0.02 10) Naphthalene-d8 15.86 136 1703230 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.15 164 977317 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.60 188 1495646 20.00 ug/1 -0.02 39) Chrysene-dl2 33.66 240 989725 20.00 ug/1 -0.02 45) Perylene-dl2 37.88 264 592553 20.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = , 0.00%

Target Compounds 2) N-nitroso-dimethyl amine 5.87 74 741133 40-0f 72.80 ug/1 Qvalue 97 3) bis(2-Chloroethyl)ether 11.63 93 1147207 72.41 ug/1 98 4) 1,3-Dichlorobenzene 12.12 146 1290385 78.98 ug/1 99 5) 1,4-Dichlorobenzene 12.26 146 1310830 79.73 ug/1 98 6) 1,2-Dichlorobenzene 12.78 146 1215470 79.61 ug/1 99 7) 2,21-oxybis(1-Chloropropan 13.10 45 1510124 68.99 ug/1 97 8) N-Nitroso-di-n-propylamine 13.51 70 743573 71.56 ug/1 98 9) Hexachloroethane 13.63 117 459627 76.30 ug/1 90 11) Nitrobenzene 13.91 77 1118512 74.90 ug/1 99 12) Isophorone 14.56 82 2113902 74.82 ug/1 99 13) bis(2-Chloroethoxy)methane 15.23 93 1386718 75.35 ug/1 99 14) 1,2,4-Trichlorobenzene 15.74 180 1087808 84.02 ug/1 99 15) Naphthalene 15.91 128 3217869 78.58 ug/1 100 16) Hexachlorobutadiene 16.45 225 563820 87.07 ug/1 99 18) Hexachlorocyclopentadiene 18.64 237 403993 93.46 ug/1 98 19) 2-Chloronaphthalene 19.42 162 2032654 78.86 ug/1 98 20) Dimethylphthalate 20.51 163 2366964 79.66 ug/1 99 21) 2,6-Dinitrotoluene 20.73 165 572196 80.54 ug/1 96 22) Acenaphthylene 20.69 152 2841815 78.81 ug/1 100 23) Acenaphthene 21.25 153 2012561 78.51 ug/1 100 24) 2,4-Dinitrotoluene 21.90 165 743535 79.50 ug/1 98 25) Diethylphthalate 22.65 149 2229646 78.23 ug/1 100 26) 4-Chlorophenyl-phenylether 22.80 204 1050503 83.07 ug/1 97 27) Fluorene 22.78 166 2188618 80.63 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.27 77 2180858 72.31 ug/L 96 31) N-Nitrosodiphenylamine 23.19 168 977183 78.54 ug/1 99 32) 4-Bromophenyl-phenylether 24.26 248 606160 83.48 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0412.M Wed Apr 24 11:13:20 2002 Page 1

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