GCMS calibration data for sample AE08971, April 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR2 502\CAL5 0A.D Vial: 2 Acq On 26 Apr 2002 10:53 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 12:38 2002 Quant Results File: GCMS0412 .RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.22 152 727801 20.00 ug/1 -0.02 10) Naphthalene-d8 15.86 136 2719105 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.16 164 1574261 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.60 188 2429905 20.00 ug/1 -0.02 39) Chrysene-dl2 33.66 240 1664250 20.00 ug/1 -0.02 45) Perylene-dl2 37.89 264 1055641 20.00 ug/1 -0.03

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine . 5.87 74 733341 46.30 ug/1 96 3) bis(2-Chloroethyl)ether 11.65 93 1128971 45.79 ug/1 98 4) 1,3-Dichlorobenzene 12.12 146 1257810 49.47 ug/1 99 5) 1,4-Dichlorobenzene 12.27 146 1262993 49.37 ug/1 100 6) 1,2-Dichlorobenzene 12.78 146 1182242 49.76 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.11 45 1470767 43.18 ug/1 96 8) N-Nitroso-di-n-propylamine 13.52 70 746047 46.14 ug/1 97 9) Hexachloroethane 13.63 117 453419 48.37 ug/1 93 11) Nitrobenzene 13.92 77 1120411 47.00 ug/1 97 12) Isophorone 14.57 82 2131019 47.24 ug/1 98 13) bis(2-Chloroethoxy)methane 15.24 93 1386110 47.18 ug/1 99 14) 1,2,4-Trichlorobenzene 15.74 180 1086933 52.58 ug/1 99 15) Naphthalene 15.91 128 3234532 49.48 ug/1 100 16) Hexachlorobutadiene 16.46 225 558222 54.00 ug/1 98 18) Hexachiorocyc1opentadiene 18.64 237 432714 62.15 ug/1 100 19) 2-Chloronaphthalene 19.42 162 2065462 49.75 ug/1 98 20) Dimethylphthalate 20.51 163 2410152 50.35 ug/1 99 21) 2,6-Dinitrotoluene 20.73 165 587507 51.34 ug/1 96 2 2) Acenaphthylene 20.69 152 2907652 50.06 ug/1 100 23) Acenaphthene 21.26 153 2053877 49.74 ug/1 99 24) 2,4-Dinitrotoluene 21.90 165 770165 51.12 ug/1 98 25) Diethylphthalate 22.66 149 2282333 49.71 ug/1 99 26) 4-Chlorophenyl-phenylether 22.79 204 1063746 52.22 ug/1 99 27) Fluorene 22.78 166 2226714 50.93 ug/1 99 2 9) Azobenzen/ 1,2-Diphenylhyd 23.27 77 2184859 44.97 ug/L 95 31) N-Nitrosodiphenylamine 23.20 168 1005359 49.74 ug/1 97 32) 4-Bromophenyl-phenylether 24.26 248 628020 53.24 ug/1 96 (#) = qualifier out of range (m) = manual integration CAL50A.D GCMS0412.M Fri Apr 26 12:38:36 2002 Page 1

NYC-WTC_000049409