GCMS calibration data AE08209, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR1702\C .D Vial: 2 Acq On 17 Apr 2002 9:10 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 15:32 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.22 152 506979 20.00 ug/1 -0.02 10) Naphthalene-d8 15.84 136 1802125 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1044093 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 1528710 20.00 ug/1 -0.02 39) Chrysene-dl2 33.64 240 992002 20.00 ug/1 -0.03 45) Perylene-dl2 37.88 264 658811 20.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds (7,5 Qvalue 2) N-nitroso-dimethyl amine 5.86 74 204048 18.49 ug/1 99 3) bis(2-Chloroethyl)ether 11.62 93 325161 18.93 ug/1 99 4) 1,3-Dichlorobenzene 12.12 146 356289 20.12 ug/1 99 5) 1,4-Dichlorobenzene 12.25 146 361820 20.30 ug/1 99 6) 1,2-Dichlorobenzene 12.78 146 338767 20.47 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.09 45 432422 18.23 ug/1 98 8) N-Nitroso-di-n-propylamine 13.48 70 203109 18.03 ug/1 98 9) Hexachloroethane 13.62 117 126263 19.34 ug/1 94 11) Nitrobenzene 13.90 77 312586 19.78 ug/1 98 12) Isophorone 14.54 82 581610 19.45 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 384451 19.74 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 298009 21.75 ug/1 98 15) Naphthalene 15.90 128 903354 20.85 ug/1 100 16) Hexachlorobutadiene 16.45 225 152368 22.24 ug/1 98 18) Hexachlorocyclopentadiene 18.64 237 82344 17.83 ug/1 99 19) 2-Chloronaphthalene 19.41 162 553886 20.11 ug/1 99 20) Dimethylphthalate 20.50 163 634030 19.97 ug/1 99. 21) 2,6-Dinitrotoluene 20.71 165 142910 18.83 ug/1 97 22) Acenaphthylene 20.67 152 762676 19.80 ug/1 99 23) Acenaphthene 21.24 153 554808 20.26 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 176808 17.70 ug/1 97 25) Diethylphthalate 22.63 149 593580 19.49 ug/1 100 26) 4-Chlorophenyl-phenylether 22.78 204 290416 21.50 ug/1 96 27) Fluorene 22.76 166 602824 20.79 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 570960 17.72 ug/L 95 31) N-Nitrosodiphenylamine 23.18 168 259227 20.39 ug/1 95 32) 4-Bromophenyl-phenylether 24.24 248 160000 21.56 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL20.D GCMS0412.M Thu Apr 18 12:48:02 2002 Page 1

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