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GCMS calibration results, April 23, 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.

NYC-WTC_000048996–000048999

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR2202\CAL80.D Vial: 2 Acq On 22 Apr 2002 9:25 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 14:49 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.69 284 663825 86.13 ug/1 96 3 4) Phenanthrene 25.67 178 2757913 79.58 ug/1 99 35) Anthracene 25.81 178 2755428 80.84 ug/1 100 36) Di-n-butylphthalate 27.57 149 3366890 77.66 ug/1 100 37) Fluoranthene 29.29 202 2791341 80.08 ug/1 96 4 0) Pyrene 29.96 202 2817360 76.28 ug/1 98 41) Butylbenzylphthalate 32.09 149 1294369 71.67 ug/1 96 42) Benzo(a)anthracene 33.60 228 2036192 79.48 ug/1 100 43) Bis(2-ethylhexyl)phthalate 33.87 149 1589171 68.77 ug/1 99 44) Chrysene 33.74 228 1999438 78.70 ug/1 100 46) Di-n-Octylphthalate 35.61 149 2372463 70.11 ug/1 # 98 47) Benzo(b)fluoranthene 36.71 252 1825800 83.51 ug/1 98 48) Benzo(k)fluoranthene 36.78 252 1728001 81.16 ug/1 99 49) Benzo(a)pyrene 37.69 252 1508680 83.70 ug/1 99 50) Indeno(l,2,3-cd)pyrene 41.98 276 1416450m 78.04 ug/1 51) Dibenz(a,h)anthracene 42.05 278 1100056 79.49 ug/1 97 52) Benzo(g,h,i)perylene 43.22 276 1104435 72.90 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0412.M Tue Apr 23 10:11:03 2002 Page 2

NYC-WTC_000048998

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NYC-WTC_000048998Source: NYC Law Department, mirrored locally

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