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GCMS calibration verification data for sample AE06981, April 2002

Machine-extracted title · confidence 100%

Calibration report for GCMS analysis listing response factors and detection limits for various organic compounds.

NYC-WTC_000060698–000060701

Folder label: “GCMS X 3/25/02 A 4/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR18 0 2\CAL2 0.D Vial: 2 Acq On 18 Apr 2002 12:30 pm Operator : Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 8:15 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.69 284 252322 22.35 ug/1 95 34) Phenanthrene 25.66 178 1037749 . 20.45 ug/1 . 100 35) Anthracene 25.79 178 1012826 20.29 ug/1 99 36) Di-n-butylphthalate 27.56 149 1192910 18.79 ug/1 100 37) Fluoranthene 29.28 202 1035567 20.28 ug/1 95 40) Pyrene 29.96 202 1041199 21.25 ug/1 94 41) Butylbenzylphthalate 32.09 149 422104 17.62 ug/1 94 42) Benzo(a)anthracene 33.59 228 680114 20.01 ug/l 100 43) Bis(2-ethylhexyl)phthalate 33.86 149 489833 15.98 ug/1 99 44) Chrysene 33.72 228 684939 20.33 ug/l 99 46) Di-n-Octylphthalate 35.60 149 660222 14.66 ug/1 # 98 47) Benzo(b)fluoranthene 36.70 252 548964 18.87 ug/1 97 48) Benzo(k)fluoranthene 36.76 252 607639 21.45 ug/1 98 49) Benzo(a)pyrene 37.68 252 468371 19.53 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.96 276 465576 19.28 ug/1 93 51) Dibenz(a,h)anthracene 42.03 278 369538 20.07 ug/1 97 52) Benzo(g,h,i)perylene 43.18 276 387023 19.20 ug/1 98

(#) = qualifier out of range (m) = manual integration CAL20.D GCMS0412.M Fri Apr 19 08:24:46 2002 Page 2

NYC-WTC_000060700

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NYC-WTC_000060700Source: NYC Law Department, mirrored locally

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