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GCMS calibration data for sample CAL20, April 2002

Machine-extracted title · confidence 90%

Calibration table excerpt from GCMS analysis of sample CAL20 showing surrogate recovery data from April 18, 2002.

NYC-WTC_000043530–000043535

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR18 02\CAL2 0A.D Vial: 2 Acq On 19 Apr 2002 1:41 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 15:20 2002 Quant Results File: GCMS0419.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.68 284 393199 23.09 ug/1 98 34) Phenanthrene 25.67 178 1585803 20.71 ug/1 99 35) Anthracene 25.80 178 1546187 20.53 ug/1 100 36) Di-n-butylphthalate 27.56 149 1884154 19.67 ug/1 99 37) Fluoranthene 29.28 202 1598143 20.75 ug/1 94 4 0) Pyrene 29.95 202 1622031 19.71 ug/1 96 41) Butylbenzylphthalate 32.08 149 716598 17.81 ug/1 99 42) Benzo(a)anthracene 33.60 228 1182181 20.71 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.87 149 874236 16.98 ug/1 97 44) Chrysene 33.73 228 1154103 20.39 ug/1 100 46) Di-n-Octylphthalate 35.61 149 1295524 15.50 ug/1 # 98 47) Benzo(b)fluoranthene 36.70 252 1067811 19.77 ug/1 98 48) Benzo(k)fluoranthene 36.78 252 1059638 20.15 ug/1 97 49) Benzo(a)pyrene 37.68 252 894642 20.09 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.97 276 879764 19.62 ug/1 95 51) Dibenz(a,h)anthracene 42.04 278 696157 20.36 ug/1 97 52) Benzo(g,h,i)perylene 43.20 276 699941 18.70 ug/1 97

(#) = qualifier out of range (m) = manual integration CAL20A.D GCMS0419.M Fri Any 19 15.21.16 000 D a Pe 2

NYC-WTC_000043534

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NYC-WTC_000043534Source: NYC Law Department, mirrored locally

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