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GCMS calibration results for sample AE07486, April 2002

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DEP laboratory report showing GCMS calibration results for sample AE07486 conducted on April 19, 2002.

NYC-WTC_000047089–000047092

Folder label: “GCMS X 4/1/02 A 4/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR1802\CAL10.D Vial: 2 Acq On 19 Apr 2002 6:34 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 10:26 2002 Quant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.68 284 99445 11.78 ug/1 # 92 34) Phenanthrene 25.65 178 404310 10.65 ug/1 99 35) Anthracene 25.79 178 385600 10.33 ug/1 100 36) Di-n-butylphthalate 27.56 149 434249 9.15 ug/1 100 37) Fluoranthene 29.27 202 379984 9.95 ug/1 97 40) Pyrene 29.95 202 390740 9.80 ug/1 95 41) Butylbenzylphthalate 32.08 149 147939 7.58 ug/1 96 42) Benzo(a)anthracene 33.59 228 261608 9.46 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 179292 7.18 ug/1 99 44) Chrysene 33.71 228 284910 10.38 ug/1 99 46) Di-n-Octylphthalate 35.60 149 224632 5.91 ug/1 99 47) Benzo(b)fluoranthene 36.69 252 221084 9.00 ug/1 98 48) Benzo(k)fluoranthene 36.76 252 257545 10.76 ug/1 97 49) Benzo(a)pyrene 37.67 252 187405 9.25 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.94 276 165691 8.12 ug/1 93 51) Dibenz(a,h)anthracene 42.03 278 126986 8.16 ug/1 # 95 52) Benzo(g,h,i)perylene 43.16 276 136833 8.04 ug/1 96

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS0419.M Mon Apr 22 12:09:41 2002 Page 2

NYC-WTC_000047091

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