GCMS calibration results for sample AE07486, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C : \HPCHEM\ 1 \DATA\APR18 02 \CAL10). D Vial: 2 Acq On 19 Apr 2002 6:34 pm / Operator : Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 10:26 2002 Quant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.22 152 479769 20.00 ug/1 -0.02 10) Naphthalene-d8 15.84 136 1744603 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 989238 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 1469324 20.00 ug/1 -0.02 39) Chrysene-dl2 33.64 240 992825 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 643832 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds 9 (3 Qvalue 2) N-nitroso-dimethyl amine 5.86 74 93980 9.00 ug/1 99 3) bis(2-Chloroethyl)ether 11.62 93 159286 9.80 ug/1 100 4) 1,3-Dichlorobenzene 12.12 146 175023 10.44 ug/1 98 5) 1,4-Dichlorobenzene 12.25 146 175237 10.39 ug/1 98 6) 1,2-Dichlorobenzene 12.78 146 166167 10.61 ug/1 98 7) 2,21-oxybis(1-Chloropropan 13.09 45 206156 9.18 ug/1 98 8) N-Nitroso-di-n-propylamine 13.48 70 94952 8.91 ug/1 97 9) Hexachloroethane 13.62 117 61736 9.99 ug/1 97 11) Nitrobenzene 13.90 77 154342 10.09 ug/1 98 12) Isophorone 14.54 82 274828 9.50 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 185014 9.81 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 146084 11.01 ug/1 99 15) Naphthalene 15.90 128 439524 10.48 ug/1 99 16) Hexachlorobutadiene 16.45 225 75935 11.45 ug/1 98 18) Hexachlorocyclopentadiene 18.64 237 42666 9.75 ug/1 99 19) 2-Chloronaphthalene 19.41 162 272902 10.46 ug/1 98 20) Dimethylphthalate 20.49 163 301666 10.03 ug/1 98 21) 2,6-Dinitrotoluene 20.71 165 62607 8.71 ug/1 95 2 2) Acenaphthylene 20.67 152 362988 9.95 ug/1 99 23) Acenaphthene 21.24 153 272594 10.51 ug/1 100 24) 2,4-Dinitrotoluene 21.87 165 82914 8.76 ug/1 98 25) Diethylphthalate 22.63 149 283843 9.84 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 144683 11.30 ug/1 97 27) Fluorene 22.76 166 291292 10.60 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 272130 8.91 ug/L 95 31) N-Nitrosodiphenylamine 23.17 168 124656 10.20 ug/1 97 32) 4-Bromophenyl-phenylether 24.24 248 78099 10.95 ug/1 97

(#) = qualifier out of range (m) = manual integration CALIO.D GCMS0419.M Mon Apr 22 12:09:40 2002 Page 1

NYC-WTC_000047090