GCMS analysis results for sample AE06412, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR04 0 5\CAL4 0.D Vial: 2 Acq On 5 Apr 2002 10:57 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 10 11:30 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 10 10:43:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 763270 20.00 ug/1 0.00 10) Naphthalene-d8 15.90 136 2866326 20.00 ug/1 0.00 17) Acenaphthene-diO 21.20 164 1645994 20.00 ug/1 0.00 30) Phenanthrene-dlO 25.65 188 2490552 20.00 ug/1 0.00 39) Chrysene-dl2 33.71 240 1426031 20.00 ug/1 0.00 45) Perylene-dl2 37.94 264 757074 20.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.89 74 856379 41.50 ug/1 98 3) bis(2-Chloroethyl)ether 11.67 93 1348762 40.28 ug/1 99 4) 1,3-Dichlorobenzene 12.15 146 1486174 41.59 ug/1 98 5) 1,4-Dichlorobenzene 12.30 146 1486240 41.36 ug/1 100 6) 1,2-Dichlorobenzene 12.82 146 1393614 41.47 ug/1 100 7) 2,2‘-oxybis(1-Chloropropan 13.14 45 1827041 40.80 ug/1 99 8) N-Nitroso-di-n-propylamine 13.55 70 888901 41.95 ug/1 99 9) Hexachloroethane 13.66 117 548644 41.98 ug/1 99 11) Nitrobenzene 13.95 77 1318662 40.78 ug/1 98 12) Isophorone 14.60 82 2516113 41.77 ug/1 100 13) bis(2-Chloroethoxy)methane 15.28 93 1645509 41.06 ug/1 99 14) 1,2,4-Trichlorobenzene 15.78 180 1252598 41.94 ug/1 99 15) Naphthalene 15.96 128 3771970 41.33 ug/1 100 16) Hexachlorobutadiene 16.49 225 642156 42.27 ug/1 100 18) Hexachlorocyclopentadiene 18.68 237 448557 42.35 ug/1 99 19) 2-Chloronaphthalene 19.46 162 2363641 41.28 ug/1 99 20) Dimethylphthalate 20.55 163 2770704 41.88 ug/1 99 21) 2,6-Dinitrotoluene 20.77 165 662204 42.43 ug/1 97 22) Acenaphthylene 20.73 152 3330722 41.75 ug/1 99 23) Acenaphthene 21.30 153 2340981 41.27 ug/1 100 24) 2,4-Dinitrotoluene 21.94 165 860171 43.04 ug/1 98 25) Diethylphthalate 22.69 149 2614246 42.04 ug/1 100 26) 4-Chlorophenyl-phenylether 22.84 204 1198352 41.60 ug/1 96 27) Fluorene 22.82 166 2517802 41.72 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.31 77 2486136 40.43 ug/L 98 31) N-Nitrosodiphenylamine 23.24 168 1129127 41.69 ug/1 99 32) 4-Bromophenyl-phenylether 24.30 248 693230 42.33 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0408.M Wed Apr 10 11:39:48 2002 Page 1

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