GCMS reference data for sample AE06412, April 2002

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0405\REF2.D Vial: 5 Acq On 5 Apr 2002 1:56 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 10 12:03 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 10 10:43:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 12.24 152 487722 20.00 ug/1 -0.02 10) Naphthalene-d8 15.89 136 1782595 20.00 ug/1 -0.02 17) Acenaphthene-diO 21. 19 164 1001681 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.63 188 1440707 20.00 ug/1 -0.03 39) Chrysene-dl2 33.69 240 758077 20.00 ug/1 -0.03 45) Perylene-dl2 37.93 264 416548 20.00 ug/1 -0.02

System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery L0 0.00% 38) 2,4-DDD 30.71 235 75049 .5.65ug/mL 0.21 Spiked Amount 5.000 Recovery 113.00% @ole Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 81809 6.20 ug/1 98 3) bis(2-Chloroethyl)ether 11.64 93 198250 9.27 ug/1 99 4) 1,3-Dichlorobenzene 12.14 146 137767 6.03 ug/1 97 5) 1,4-Dichlorobenzene 12.29 146 149827 6.53 ug/1 98 6) 1,2-Dichlorobenzene 12.80 146 153475 7.15 ug/1 99 7) 2,2‘-oxybis(1-Chloropropan 13.13 45 271382 9.48 ug/1 98 8) N-Nitroso-di-n-propylamine 13.51 70 131125 9.69 ug/1 98 9) Hexachloroethane 13.66 117 30788 3.69 ug/1 94 11) Nitrobenzene 13.92 77 175676 8.74 ug/1 97 12) Isophorone 14.58 82 366679 9.79 ug/1 100 13) bis(2-Chloroethoxy)methane 15.26 93 237475 9.53 ug/1 99 14) 1,2,4-Trichlorobenzene 15.77 180 136767 7.36 ug/1 96 15) Naphthalene 15.94 128 506997 8.93 ug/1 99 16) Hexachlorobutadiene 16.49 225 24687 2.61 ug/1 98 18) Hexachlorocyclopentadiene 18.68 237 8109 1.26 ug/1 97 19) 2-Chloronaphthalene 19.44 162 313321 8.99 ug/1 99 20) Dimethylphthalate 20.53 163 443315 11.01 ug/1 100 21) 2,6-Dinitrotoluene 2 0.75 165 89205 9.39 ug/1 91 22) Acenaphthylene 20.72 152 487813 10.05 ug/1 100 23) Acenaphthene 21.28 153 342358 9.92 ug/1 99 24) 2,4-Dinitrotoluene 21.92 165 111005 9.13 ug/1 99 25) Diethylphthalate 22.66 149 424244 11.21 ug/1 99 26) 4-Chlorophenyl-phenylether 22.82 2 04 182646 10.42 ug/1 99 27) Fluorene 22.80 166 384055 10.46 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.29 77 354894 9.48 ug/L 98 31) N-Nitrosodiphenylamine 23.22 168 147177 9.39 ug/1 96 32) 4-Bromophenyl-phenylether 24.29 248 99409 10.49 ug/1 99

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0408.M Wed Apr 10 12:07:31 2002 Page 1

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