GCMS analysis results for sample AE06991, April 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR0405\CAL4OA.D Vial: 2 Acq On 6 Apr 2002 6:43 am 00 Operator: Sample Inst : GC S 209 Mise Multiplr: .00 MS Integration Params: GOOFY.P Quant Time: Apr 15 14:16 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 15 14:10:52 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 838348 20.00 ug/1 0.00 10) Naphthalene-d8 15.89 136 3164153 20.00 ug/1 -0.02 17) Acenaphthene-diO 21.20 164 1821688 20.00 ug/1 0.00 30) Phenanthrene-diO 25.64 188 2739254 20.00 ug/1 -0.02 . 39) Chrysene-dl2 33.71 240 1548464 20.00 ug/1 0.00 45) Perylene-dl2 37.94 264 798056 20.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds (1 • 1 Qvalue 2) N-nitroso-dimethyl amine 5.89 74 936068 82.59 ug/1 99 3) bis(2-Chloroethyl)ether 11.67 93 1483108 80.65 ug/1 99 4) 1,3-Dichlorobenzene 12.16 146 1628741 83.00 ug/1 98 5) 1,4-Dichlorobenzene 12.30 146 1639439 83.08 ug/1 99 6) 1,2-Dichlorobenzene 12.82 146 1530068 82.90 ug/1 99 7) 2,21-oxybis(1-Chloropropan 13.14 45 2001943 81.40 ug/1 100 8) N-Nitroso-di-n-propylamine 13.55 70 971043 83.45 ug/1 98 9) Hexachloroethane 13.66 117 594702 82.87 ug/1 96 11) Nitrobenzene 13.95 77 1439419 80.65 ug/1 99 12) Isophorone 14.60 82 2774432 83.45 ug/1 100 13) bis(2-Chloroethoxy)methane 15.28 93 1809148 81.79 ug/1 100 14) 1,2,4-Trichlorobenzene 15.78 180 1374801 83.40 ug/1 99 15) Naphthalene 15.96 128 4155018 82.48 ug/1 100 16) Hexachlorobutadiene 16.49 225 704877 84.06 ug11 99 18) Hexachlorocyclopentadiene 18.68 237 471428 80.43 ug/1 99 19) 2-Chloronaphthalene 19.46 162 2609894 82.37 ug/1 100 20) Dimethylphthalate 20.56 163 3044925 83.17 ug/1 100 21) 2,6-Dinitrotoluene 20.78 165 731224 84.67 ug/1 97 22) Acenaphthylene 20.73 152 3663064 82.97 ug/1 99 23) Acenaphthene 21.30 153 2567232 81.79 ug/1 99 24) 2,4-Dinitrotoluene 21.94 165 957500 86.57 ug/1 99 25) Diethylphthalate 22.70 149 . 2891131 84.01 ug/1 99 26) 4-Chlorophenyl-phenylether 22.83 204 1309756 82.16 ug/1 99 27) Fluorene 22.82 166 2771629 83.00 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.31 77 2754676 80.96 ug/L 98 31) N-Nitrosodiphenylamine 23.24 168 1225456 82.28 ug/1 99 32) 4-Bromophenyl-phenylether 24.30 248 764720 84.92 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL40A.D GCMS0408.M Mon Apr 15 14:20:00 2002 Page 1

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