GCMS reference analysis results for sample AE07311, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0302\CAL40.D Vial: 2 Acq On 3 Apr 2002 12:38 pm Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 8 10:57 2002 Quant Results File: GCMS0403.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 10:55:57 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue

27) Fluorene 22.82 166 1900550 42.09 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.30 77 1918827 41.71 ug/L 98 31) N-Nitrosodiphenylamine 23.23 168 833552 41.06 ug/1 99 32) 4-Bromophenyl-phenylether 24.29 248 511350 41.66 ug/1 96 33) Hexachlorobenzene 24.73 284 606788 41.32 ug/1 99 34) Phenanthrene 25.71 178 2640517 41.51 ug/1 100 35) Anthracene 25.85 178 2627940 42.55 ug/1 100 36) Di-n-butylphthalate 27.61 149 3248312 42.44 ug/1 100 37) Fluoranthene 29.33 202 2633779 42.40 ug/1 100 40) Pyrene 30.01 202 2639316 42.19 ug/1 100 41) Butylbenzylphthalate 32.13 149 1176070 43.54 ug/1 98 42) Benzo(a)anthracene 33.65 228 1613661 42.56 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.91 149 1362303 43.91 ug/1 99 44) Chrysene 33.78 228 1592897 41.59 ug/1 99 46) Di-n-Octylphthalate 35.65 149 1880585 46.06 ug/1 # 99 47) Benzo(b)fluoranthene 36.76 252 1202654 42.46 ug/1 100 48) Benzo(k)fluoranthene 36.82 252 1199218 41.04 ug/1 99 4 9) Benzo(a)pyrene 37.75 252 1011368 44.03 ug/1 99 50) Indeno(1,2,3-cd)pyrene 42.07 276 912895 43.72 ug/1 99 51) Dibenz(a,h)anthracene 42.14 278 706031 43.34 ug/1 99 52) Benzo(g,h,i)perylene 43.32 276 731993 42.83 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0403.M Mon Apr 08 10:58:59 200.2 Page 2

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