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GCMS analysis results for sample AE01965, April 2002

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Laboratory report documenting GCMS analysis of sample AE01965 conducted on April 10, 2002.

NYC-WTC_000046570–000046577

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO 3 02\REF1.D Vial: 4 Acq On 3 Apr 2002 3:36 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 8 11:33 2002 Quant Results File: GCMS0403.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Compound R.T. Qlon Response Cone Unit Qvalue

27) Fluorene 22.80 166 450743 13.53 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.28 77 418456 12.32 ug/L 95 31) N-Nitrosodiphenylamine 23.21 168 155571 10.87 ug/1 98 32) 4-Bromophenyl-phenylether 24.29 248 116067 13.41 ug/1 96 33) Hexachlorobenzene 24.73 284 140292 13.55 ug/1 98 34) Phenanthrene 25.70 178 623135 13.89 ug/1 100 35) Anthracene 25.83 178 558898 12.83 ug/1 100 36) Di-n-butylphthalate 27.60 149 806077 14.94 ug/1 99 37) Fluoranthene 29.33 202 590553 13.48 ug/1 99 40) Pyrene 30.00 202 609935 15.02 ug/1 99 41) Butylbenzylphthalate 32.13 149 253544 14.46 ug/1 98 42) Benzo(a)anthracene 33.64 228 340316 13.83 ug/1 100 43) Bis(2-ethylhexyl)phthalate 33.91 149 406102 20.16 ug/1 99 44) Chrysene 33.77 228 374715 15.07 ug/1 99 46) Di-n-Octylphthalate 35.65 149 328336 12.06 ug/1 # 99 47) Benzo(b)fluoranthene 36.74 252 258805 13.70 ug/1 99 48) Benzo(k)fluoranthene 36.81 252 286442 14.70 ug/1 98 4 9) Benzo(a)pyrene 37.73 252 168732 11.02 ug/1 99 50) Indeno(1,2,3-cd)pyrene 42.05 276 168997 12.14 ug/1 98 51) Dibenz(a,h)anthracene 42.12 278 147524 13.58 ug/1 98 52) Benzo(g,h,i)perylene 43.29 276 153368 13.46 ug/1 97

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0403.M Mon Apr 08 11:37:53 2002 Page 2

NYC-WTC_000046576

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NYC-WTC_000046576Source: NYC Law Department, mirrored locally

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