GCMS calibration table data, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0302\9579.D Vial: 9 Acq On 3 May 2002 9:52 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Hexanoic acid Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

11.22 1.17 ug/1 71137 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanoic acid 116 C6H1202 000142-62-1 83/ 2 Pentanoic acid 102 C5H10O2 000109-52-4—78 3 Pentanoic acid, 3-methyl- 116 C6H1202 000105-43-1 56 4 Butanoic acid, 3-methyl- 102 C5H10O2 000503-74-2 50 Abundance Scan 674 (11.218 min): 9579.D (-) m/z 60.00 100.00% 60

5000 73 41 55 87 TT8 I I I I I I I I I I I I I I ] I I I

10.80 11.00 11.20 11.40 11.60

m/z-> 36 HI 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 3 # - r 11' r 111 r " ' i " 1' i"1' i m/z 73.10 46.83% Abundance #64269: Hexanoic acid 60

5000 I 1 ' 1 1 I J ' 73 10.80 11.00 11.20 11.40 11.60 41 m/ z 41.05 30.12% 55 87 33 III I [ I I I I I > I I I [ I I I I I I-1-1 if I / LH 11 । ■ ■ ■ ■ । ■ l ■ ■ ।" I‘‘*‘IUSIIIIIN) 116 m/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #63515: Pentanoic acid 60 / i 1 ' ■ ' i 1 ' 1 1 1 1 1 1 1 ' 10.80 11.00 11.20 11.40 11.60 5000 m/ Z 43.05 20.86% 73 41 55 ... |h- 1}UT0—0n———87 m/z-> Abundance TT I'1" I " " I TH 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 #64326: Pentanoic acid, 3-methyl- 60 ku——0n—um—m—RTT IA 10.80 11.00 11.20 11.40 11.60 m/ z 55.10 17.53% 5000

/z—> 1 r1" ।" " ।" 41 > ! | I , I > I I I 55 I I I I ।

25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 + u . 73 87 I T r 1" p I I I | i i i i | i i TT I i i | i > i i | I i i i [ i r i r | r t r i | > I I I | I VT 1 | M I ' ' 1 1 I 10.80 11.00 11.20 11.40 11.60 WA t । I । j iiii । r r I

9579.D GCMS0501.M Mon May 06 10:49:51 2002 Page 4

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