GCMS calibration table data, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0302\9579.D Vial: 9 Acq On 3 May 2002 9:52 pm ' Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 5 2H-Pyran, 3,4-dihydro- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 13.83 1.25 ug/1 76012 1,4-Dichlorobenzene-d4 12.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Pyran, /3,4-dihydro- 84 C5H80 000110-87-2 38 2 3-Ethyl-2-methyl-1 -heptene 140 C10H20 019780-60-0 37 3 2-Pentenal, (E) - 84 C5H80 001576-87-0 30 4 2-Ethylacrolein__________________ 84 C5H80 000922-63-4 27 Abundance 7 Scan 959 (13.829 min): 9579.D (-) m/z 55.10 100.00% 41 55

69 5000 84

96 i 1 ' 1 11 ' ' —

+— l 13.40 13.60 13.80 14.00 14.20 111 1 11 i' 1'11 49 m/ Z 41.05 98.12% m/z->20 30 40 Abundance 50 l 80 90 100 110 120 130 140

55 60 70 #62717: 2H-Pyran, 3,4-dihydro- J 84 5000 27 13.40 13.60 13.80 14.00 14.20 m/z 69.05 60.96% 69 g ■ । • ■ ■ ■ । ■ ■ ■ < । ■ 1 1 i ' ■ 1 ■ i ■ ' ■ 1 i ' 1 ' ■ i 1 ■ ■ 1 i ■ ■ 1 1 i 1 ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #7610: 3-Ethyl-2-methyl-1 -heptene 55 69 84 ‘ ' i ' ' ■ 1 i ’ ' 13.40 13.60 13.80 14.00 14.20 5000 m/z 84.00 49.62%

27 ....... 1.............. - > l 1 ■ ■ - I ■ i ■ i [ n 97 ' ।1 ■11111 ■11 1 ‘ 111 140 i I | । । । । ] । r i । । । । । । । । । n । i i I"I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #567: 2-Pentenal, (E)- FTT 55 1340 13.60 13.80 14.00 14.20 m/ z 39.00 44.93% 27 39 84 5000

m/z--> 1 [ । > 1 । । i r 1 1 1 ’ 11 1,

20 30 40 50 .... ..... I I I I I I I I J I I I I I 60 70 80 ■ ■ । 1 1 1 1 । 1 1 1 ■ । 1 1 1 ' । ' f1 । । । । । । । । । 90 100 110 120 130 140 AU. I-1 1fr 'I ' 1 ! 1 I ' 111 I1 ' 13.40 13.60 13.80 14.00 14.20

9579.D GCMS0501.M Mon May 06 10:49:52 2002 Page 5

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