GCMS calibration table data, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C : \HPCHEM\ 1 \DATA\MAYO 302\9579.D Vial: 9 Acq On 3 May 2002 9 : 52, pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 2-Propanone, 1-cyclopropyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 9.96 0.57 ug/1 34505 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 entative ID MW MolForm CAS# Qual

1 2-Propanone, 1-cyclopropyl- 98 C6H10O 004160-75-2 9 2 3-Oxetanol/ 2,2,3-trimethyl- 116 C6H1202 025910-96-7 9 3 2-Hexanone, 4-methyl- 114 C7H140 000105-42-0 9 4 Hydroperoxide, 1-methylethyl 76 C3H802 003031-75-2 9 Abundance Scan 537 (9.962 min): 9579. D (-) m/ z 43.05 100.00% 43

5000 58 87 + > । । ■ i - । 35 ■ i - ■ 11 ■ 1 98 9.60 9.80 10.00 10.20 1/* m/ z 58.10 23.72% m/z->____ 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1306: 2-Propanone, 1 -cyclopropyl- 43

5000- 9.60 9.80 10.00 10.20 A—N, , 55 m/ z 59.10 17.49% 29 83 98 ----- 1..1.. 99. 1 1 i 11 1 1 i 1 1 ' h 1-1 II ■[ । । । । । । m/z-> 10 20 30 40 50 60 80 70 90 100 110 120 Abundance #3281:3-Oxetanol, 2,2,3-trimethyl- 43 । 1 1,1 । 1 9.60 9.80 10.00 10.20 5000 m/ z 87.05 14.68%I 58 71 27 86

1 ' i 1 1 1 1 I 1 11 J. I... ..... . ............ I I I ' I I I I I I I I [ ‘ I I ■ I I I I I I I I I k I I I I I I m/z—>____ 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3066: 2-Hexanone, 4-methyl- ' । । ' । 3 r- t । ~i । [ i i i i "| i 43 9.60 9.80 10.00 10.20 m/ z 42.05 10.21%| 58 5000-

AADaa 15 27 ,,, I.. 1 i ' 1 ' ' i 1 1 । ' । 1 1 1 1 i ' 1 1 I ' 1,11 | 71 85 99 114 | I I I I TT1 I I I 1 I I I ! I I I I I I I I I—I—I—I—I—T m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 9.60 9.80 10.00 10.20

9579.D GCMS0501.M Mon May 06 10:49:50 2002 Page 3

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